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Chemical Structure| 42404-09-1 Chemical Structure| 42404-09-1

Structure of 42404-09-1

Chemical Structure| 42404-09-1

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Product Details of [ 42404-09-1 ]

CAS No. :42404-09-1
Formula : C9H11NO2
M.W : 165.19
SMILES Code : O=C(N(C)C1=CC=CC=C1)CO
MDL No. :MFCD03265375

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Application In Synthesis of [ 42404-09-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 42404-09-1 ]

[ 42404-09-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 3621-82-7 ]
  • [ 42404-09-1 ]
  • 2-(6-chlorobenzoxazol-2-yl)-N-methyloxyacetanilide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; In isopropyl alcohol; EXAMPLE 2 STR55 A solution of 9.4 g (0.05 mole) of <strong>[3621-82-7]2,6-dichlorobenzoxazole</strong> in 20 ml of isopropanol is added dropwise to a mixture of 8.2 g (0.05 mole) of glycolic acid N-methylanilide and 3.1 g (0.05 mole) of powdered potassium hydroxide in 80 ml of isopropanol at -10° C., with stirring, and, when the addition has ended, the mixture is stirred at -5° C. for a further 15 hours. For working up, the reaction mixture is poured into water and the solid precipitate is filtered off with suction, rinsed with water and dried. 13 g (82percent of theory) of 2-(6-chlorobenzoxazol-2-yl)-N-methyloxyacetanilide of melting point 139° C. are obtained. The following compounds of the general formula (I) are obtained in a corresponding manner and in accordance with the general preparation statements.
 

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