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Chemical Structure| 42899-83-2 Chemical Structure| 42899-83-2

Structure of 42899-83-2

Chemical Structure| 42899-83-2

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Product Details of [ 42899-83-2 ]

CAS No. :42899-83-2
Formula : C14H8ClNO2
M.W : 257.67
SMILES Code : O=C1N(C2=CC=CC=C2)C(C3=C1C=CC=C3Cl)=O

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Application In Synthesis of [ 42899-83-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 42899-83-2 ]

[ 42899-83-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 117-21-5 ]
  • [ 62-53-3 ]
  • [ 42899-83-2 ]
YieldReaction ConditionsOperation in experiment
In acetic acid; for 3h;Reflux; SYNTHESIS EXAMPLE 105-1 An acetic acid (200 mL) solution of <strong>[117-21-5]3-chlorophthalic anhydride</strong> (36.5 g) and aniline (18.6 g) was heated to reflux for 3 hours. After cooling to room temperature, the reaction mixture was poured into iced water, and the precipitated crystal was collected by filtration, washed with water and 5% isopropanol aqueous solution, and then dried. The resulting crude crystal was washed with a t-butylmethylether/petroleum ether mixed solvent to obtain 3-chloro-N-phenylphthalimide (50.1 g). 1H-NMR (CDCl3, δ ppm): 7.38-7.55 (5H, m), 7.69-7.74 (2H, m), 7.85-7.91 (1H, m).
 

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