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Chemical Structure| 462066-71-3 Chemical Structure| 462066-71-3

Structure of 462066-71-3

Chemical Structure| 462066-71-3

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Product Details of [ 462066-71-3 ]

CAS No. :462066-71-3
Formula : C5H6N6S
M.W : 182.21
SMILES Code : SC1=NC2=C(N)N=C(N)N=C2N1
MDL No. :MFCD01002844

Safety of [ 462066-71-3 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 462066-71-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 462066-71-3 ]

[ 462066-71-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 462066-71-3 ]
  • [ 3032-81-3 ]
  • 8-((3,5-dichlorophenyl)thio)-9H-purine-2,6-diamine [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% With copper(l) iodide; 2.9-dimethyl-1,10-phenanthroline; sodium t-butanolate; In N,N-dimethyl-formamide; at 110℃; for 20h;Inert atmosphere; Sealed tube; 2,6-diamino-9H-purine-8- thiol (3.6 mmol), neocuproine hydrate (0.36 mmol), Cul (0.36 mmol), NaO-?-Bu (7.2 mmol), 1,3- dichloro-5-iodobenzene (10.8 mmol), and anhydrous DMF (24 mL) were taken in a round bottom flask flushed with nitrogen. The flask was sealed with Teflon tape, heated at 1 10 °C, and magnetically stirred for 20 h under nitrogen. Solvent was removed under reduced pressure and the resulting residue was chromatographed (CH2Cl2:MeOH:AcOH, 20: 1 :0.5). Obtained as a light yellow solid in 65 percent yield. MS (ESI): m/z 326.9 [M + H]+.
 

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