Home Cart Sign in  
Chemical Structure| 4913-77-3 Chemical Structure| 4913-77-3

Structure of 4913-77-3

Chemical Structure| 4913-77-3

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 4913-77-3 ]

CAS No. :4913-77-3
Formula : C13H10ClNO
M.W : 231.68
SMILES Code : O=C(C1=CC=C(N)C=C1)C2=CC=C(Cl)C=C2
MDL No. :MFCD01244946

Safety of [ 4913-77-3 ]

Application In Synthesis of [ 4913-77-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 4913-77-3 ]

[ 4913-77-3 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 61929-24-6 ]
  • [ 4913-77-3 ]
  • [ 1562690-64-5 ]
YieldReaction ConditionsOperation in experiment
18% With toluene-4-sulfonic acid; In isopropyl alcohol; [0205] Step 3. To a solution of Compound 9-D (0.2 g, 0.86 mmol) in isopropanol (9 mL) was added Compound 9-E (0.14 g, 0.86 mmol) and p-toluenesulfonic acid (0.16 g, 0.86 mmol). Then the mixture was refluxed overnight. Monitoring by thin layer chromatography (petroleum ether/ethyl acetate=4: 1 and Rf at 0.2) showed the reaction was almost complete. The solvent was removed. The residue was purified by silica gel chromatography and preparative HPLC to give the title compound (181 mg, combined with other 2 batches, yield = 18 %) as a yellow solid. ?H NMR (400 MHz, DMSO) oe 8.64 (s, J= 8 Hz, 1H), 7.66-7.61 (m, 4H), 7.57-7.53 (m, 4H). MS: 316.0 (M+lj.
 

Historical Records

Technical Information

• Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chan-Lam Coupling Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Lawesson's Reagent • Leuckart-Wallach Reaction • Mannich Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Ketenes • Specialized Acylation Reagents-Vilsmeier Reagent • Stille Coupling • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

Categories