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Chemical Structure| 49662-17-1 Chemical Structure| 49662-17-1

Structure of 49662-17-1

Chemical Structure| 49662-17-1

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Product Details of [ 49662-17-1 ]

CAS No. :49662-17-1
Formula : C18H14N2
M.W : 258.32
SMILES Code : C12N(C3C=CC=CC=3)C3C=CC=CC=3NC1=CC=CC=2
MDL No. :N/A

Safety of [ 49662-17-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 49662-17-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 49662-17-1 ]

[ 49662-17-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 49662-17-1 ]
  • [ 3029-64-9 ]
  • C59H39N9 [ No CAS ]
YieldReaction ConditionsOperation in experiment
55.8% 9.00 g (35 mmol) of 10-phenylphenol azine was added to a 250 ml three-necked flask, and 100 ml of N,N-dimethylformamide was added as a reaction solvent under ice bath conditions.Stir on a magnetic stirrer for 10 min. 0.72 g (30 mmol) of NaH was added portionwise to the reaction flask and stirring was continued for 1 h.2.07 g (10 mmol) of <strong>[3029-64-9]2,4,6-trichloro-5-cyanopyrimidine</strong> was dissolved in 40 ml of N,N-dimethylformamide solution, and added dropwise to the reaction system. After the addition, at room temperature The reaction was carried out for 24 h. After the reaction was completed, the reaction solution was poured into 200 ml of 10percent diluted hydrochloric acid, and the mixture was filtered under reduced pressure, washed with water and dried, and the crude product was obtained from petroleum ether and dichloromethane (PE: DCM=10: 1) Pass the column for the mobile phase. 4.87 g of a white solid powder was obtained in a yield of 55.8percent.
 

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