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Chemical Structure| 5028-25-1 Chemical Structure| 5028-25-1

Structure of 5028-25-1

Chemical Structure| 5028-25-1

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Product Details of [ 5028-25-1 ]

CAS No. :5028-25-1
Formula : C7H11N3
M.W : 137.18
SMILES Code : NC1=CC=CN=C1N(C)C
MDL No. :MFCD09737533

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Application In Synthesis of [ 5028-25-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5028-25-1 ]

[ 5028-25-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 464213-93-2 ]
  • [ 5028-25-1 ]
  • [ 37091-73-9 ]
  • N-(2-Dimethylaminopyridin-3-yl)-5-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-yl)methyl-2-acetoxybenzamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With triethylamine; In dichloromethane; Example 217 N-(2-Dimethylaminopyridin-3-yl)-5-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-yl)methyl-2-acetoxybenzamide 3-Amino-2-dimethylaminopyridine (0.154 g, 1.125 mmol), triethylamine (0.114 g, 1.125 mmol) and <strong>[37091-73-9]2-chloro-1,3-dimethylimidazolinium chloride</strong> (0.190 g, 1.125 mmol) were added to a methylene chloride solution (100 ml) of 5-(5,6-dimethoxy-3-methyl-1,4-benzoquinon-2-yl)methyl-2-acetoxybenzoic acid (0.281 g, 0.750 mmol) and the resulting solution was stirred at room temperature for 4 hours. The reaction solution was poured into ice water and then extracted with methylene chloride. The extract was washed with water and then dried, and the solvent was removed by distillation. The obtained residue was purified by preparative thin-layer chromatography (chloroform: methanol = 95:5) to obtain the titled compound (0.139 g, 0.282 mmol, 38percent).
 

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