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Chemical Structure| 504437-66-5 Chemical Structure| 504437-66-5

Structure of 504437-66-5

Chemical Structure| 504437-66-5

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Product Details of [ 504437-66-5 ]

CAS No. :504437-66-5
Formula : C18H24BFN2O5
M.W : 378.20
SMILES Code : CC(NC[C@H]1CN(C2=CC=C(B3OC(C)(C)C(C)(C)O3)C(F)=C2)C(O1)=O)=O

Safety of [ 504437-66-5 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 504437-66-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 504437-66-5 ]

[ 504437-66-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 504437-66-5 ]
  • [ 24078-12-4 ]
  • (S)-N-(3-((2-fluoro-3'-methyl-40-formyl)biphenyl-4-yl)-2-oxo-1,3-oxazolidine-5-ylmethyl)acetamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
84% With bis-triphenylphosphine-palladium(II) chloride; In water; N,N-dimethyl-formamide; at 75℃; for 10h;Alkaline conditions; Inert atmosphere; General procedure: To a well-stirred solution of intermediate 4 (2.0 g, 5.29 mmol)and sodium carbonate (2.24 g, 21.16 mmol) in DMF (20 mL) andwater (2 mL) was added 4-bromo-2-hydroxybenzaldehyde (1.06 g,5.29 mmol) and Pd(PPh3)2Cl2 (0.18 g, 0.26 mmol), then the mixturewas stirred at 75 C for 10 h under nitrogen. After completion of thereaction monitored by TLC, water (50 mL) was added and themixture was extracted with DCM (15mL 3) for three times. Theorganic phase was washed with brine and concentrated in vacuo toyield 5a as a white solid in 73% yield.
 

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