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Chemical Structure| 50778-91-1 Chemical Structure| 50778-91-1

Structure of 50778-91-1

Chemical Structure| 50778-91-1

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Product Details of [ 50778-91-1 ]

CAS No. :50778-91-1
Formula : C3H5Cl2NO
M.W : 141.98
SMILES Code : O=C(Cl)N(CCl)C
MDL No. :MFCD19232377

Safety of [ 50778-91-1 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H227-H315-H318-H335
Precautionary Statements:P261-P280-P305+P351+P338
Class:8
UN#:3265
Packing Group:

Application In Synthesis of [ 50778-91-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 50778-91-1 ]

[ 50778-91-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50778-91-1 ]
  • [ 2986-17-6 ]
  • 2-Isopropylimino-3-isopropyl-5-methyl-tetrahydro-1,3,5-thiadiazin-4-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium hydroxide; In benzene; STR104 To 2.8 g (0.02 mole) of N-methyl-N-chloromethylcarbamoyl chloride dissolved in 50 ml of benzene, was added 3.2 g (0.02 mole) of <strong>[2986-17-6]1,3-diisopropylthiourea</strong>. The mixture was heated under reflux with stirring for 2 hours. After cooling, 10 g of a 30percent potassium hydroxide solution and 50 ml of benzene were added to the mixture and the mixture was shaken thoroughly. The separated benzene layer was washed with water, dried, and the benzene was distilled off under vacuum. The crystals thus obtained were recrystallized from ether. Yield 3.0 g (66percent); m.p. 76°-77° C. NMR(CDCl3)delta: 1.15(d. 6H), 1.40(d. 6H), 3.10(S. 3H) 4.45(S. 2H), 4.50-4.80(m. 1H), 3.30-3.80(m. 1H)
 

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