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Chemical Structure| 53327-14-3 Chemical Structure| 53327-14-3

Structure of 53327-14-3

Chemical Structure| 53327-14-3

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Product Details of [ 53327-14-3 ]

CAS No. :53327-14-3
Formula : C11H12O2
M.W : 176.21
SMILES Code : CC(C1=CC=CC=C1OCC=C)=O
MDL No. :MFCD00026218

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Application In Synthesis of [ 53327-14-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53327-14-3 ]

[ 53327-14-3 ] Synthesis Path-Downstream   1~2

  • 2
  • [ 53327-14-3 ]
  • [ 1195-33-1 ]
  • 3-(((4-bromophenyl)sulfonyl)methyl)chroman-4-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
70% With dipotassium peroxodisulfate; eosin Y disodium salt; In water; N,N-dimethyl-formamide; at 20℃; for 24h;Irradiation; General procedure: A sealable reaction tube equipped with a magnetic stirrer bar was charged with 2-(allyloxy)benzaldehyde (0.2mmol), benzenesulfinic acid (3.0 equiv.), Na2-Eosin Y (4 mol%), K2S2O8 (3.0 equiv.), DMF:H2O=1:1 (2 ml), 8W blue. The reaction vessel was carried out room temperature. After completion, it was diluted with ethylacetate, washed with water. After the solvent was removed under reduced pressure, the residue was purified bycolumn chromatography on silica gel to afford the corresponding product.
 

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