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Type HazMat fee for 500 gram (Estimated)
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Chemical Structure| 534-08-7 Chemical Structure| 534-08-7

Structure of 534-08-7

Chemical Structure| 534-08-7

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Product Details of [ 534-08-7 ]

CAS No. :534-08-7
Formula : C3H6I2O
M.W : 311.89
SMILES Code : OC(CI)CI
MDL No. :MFCD01696987

Safety of [ 534-08-7 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H226-H301-H315-H319-H335-H351
Precautionary Statements:P201-P202-P210-P233-P240-P241-P242-P243-P261-P264-P270-P271-P280-P301+P310+P330-P303+P361+P353-P304+P340+P312-P305+P351+P338-P308+P313-P332+P313-P337+P313-P370+P378-P403+P233-P403+P235-P405-P501
Class:3(6.1)
UN#:1992
Packing Group:

Application In Synthesis of [ 534-08-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 534-08-7 ]

[ 534-08-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 534-08-7 ]
  • [ 75-50-3 ]
  • [ 123-47-7 ]
YieldReaction ConditionsOperation in experiment
23.5 g In ethanol; at 30 - 60℃; for 3.0h; (2) 80mL of 33% trimethylamine ethanol solution was added in the 250mL reaction flask by weight percentage,31.2 g (0.1 mol) of 1,3-diiodo-2-propanol was added dropwise at 20-30 C, and the temperature was raised to 60 C for 3 h after the dropwise addition, and a large amount of white solid appeared. Cooled to 0-5 C., filtered, washed with a small amount of ethanol, and dried in vacuo to obtain 30.5 g of a crude prodromium iodide product with a yield of 70.9%.(3) This crude product was recrystallized with 183 g of ethanol to obtain 23.5 g of the finished product of proammonium iodide. The purity was 98.05% as detected by ion chromatography.
 

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