Home Cart Sign in  
Chemical Structure| 5369-21-1 Chemical Structure| 5369-21-1

Structure of 5369-21-1

Chemical Structure| 5369-21-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 5369-21-1 ]

CAS No. :5369-21-1
Formula : C12H17N
M.W : 175.27
SMILES Code : NC1=CC=CC(C2CCCCC2)=C1
MDL No. :MFCD11899181
InChI Key :KKHJTHLWDZQCFP-UHFFFAOYSA-N
Pubchem ID :11321261

Safety of [ 5369-21-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501

Application In Synthesis of [ 5369-21-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5369-21-1 ]

[ 5369-21-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1171919-75-7 ]
  • [ 5369-21-1 ]
  • [ 2365-48-2 ]
  • [ 530-62-1 ]
  • methyl 5-(3-cyclohexylphenyl)-4-oxo-4,5-dihydro-3H-1-thia-3,5,8-triazaacenaphthylene-2-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
36.5% A solution of 2-chloro-4-iodo-pyridine-3-carbonitrile (1.60 g, 6.05 mmol), 3-cyclohexylaniline (1.06, 6.05 mmol), Pd(OAc)2(134 mg, 0.600 mmol), DPEphos (646 mg, 1.20 mmol), and Cs2C03(3.93 g, 12.1 mmol) in dioxane (100 mL) was heated at reflux under N2overnight. Methyl 2-sulfanylacetate (0.955 g, 9.00 mmol) was added and stirred at reflux overnight. CDI (2.92 g, 18.0 mmol) was added and stirred at reflux overnight. The reaction mixture was concentrated to dryness and the residue was purified by flash column chromatography to give the title compound as a pale yellow solid (900 mg, 36.5% yield).
  • 2
  • [ 1171919-75-7 ]
  • [ 5369-21-1 ]
  • [ 530-62-1 ]
  • methyl 5-(3-cyclohexylphenyl)-4-oxo-4,5-dihydro-3H-1-thia-3,5,8-triazaacenaphthylene-2-carboxylate [ No CAS ]
YieldReaction ConditionsOperation in experiment
36.5% A solution of 2-chloro-4-iodo-pyridine-3-carbonitrile (1.60 g, 6.05 mmol) , 3-cyclohexylaniline (1.06, 6.05 mmol) , Pd (OAc)2(134 mg, 0.600 mmol) , DPEphos (646 mg, 1.20 mmol) , and Cs2CO3(3.93 g, 12.1 mmol) in dioxane (100 mL) was heated at reflux under N2overnight. Methyl 2-sulfanylacetate (0.955 g, 9.00 mmol) was added and stirred at reflux overnight. CDI (2.92 g, 18.0 mmol) was added and stirred at reflux overnight. The reaction mixture was concentrated to dryness and the residue was purified by flash column chromatography to give the title compound as a pale yellow solid (900 mg, 36.5yield) .
 

Historical Records

Technical Information

Categories