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Chemical Structure| 53911-69-6 Chemical Structure| 53911-69-6

Structure of 53911-69-6

Chemical Structure| 53911-69-6

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Product Details of [ 53911-69-6 ]

CAS No. :53911-69-6
Formula : C11H9NO5
M.W : 235.19
SMILES Code : O=C1CC(C2=CC=C([N+]([O-])=O)C=C2)CC(O1)=O
MDL No. :MFCD11111096

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Application In Synthesis of [ 53911-69-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 53911-69-6 ]

[ 53911-69-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 92289-14-0 ]
  • [ 53911-69-6 ]
YieldReaction ConditionsOperation in experiment
70% With acetic anhydride; at 80℃; for 1h; b) 4-(4-Nitro-phenyl)-dihydro-pyran-2,6-dione A flask was charged with 20.0 g (79.0 mmol) of 3-(4-nitro-phenyl)-pentanedioic acid (as prepared in the previous step) and 22.4 mL (237 mmol) of acetic anhydride. The mixture was heated to 80 C. for 1 h, cooled to RT, and treated slowly with ether until the product began to precipitate. After allowing the solid to fully precipitate, the solid was filtered, washed with ether, and air-dried to afford 13.0 g (70%) of the title compound as an off-white solid: 1H-NMR (CDCl3; 400 MHz): δ 8.28 (d, 2H, J=8.8 Hz), 7.41 (d, 2H, J=8.8 Hz), 3.64-3.53 (m, 1H), 3.22-3.13 (m, 2H), 2.96-2.85 (m, 2H).
  • 2
  • [ 64-17-5 ]
  • [ 53911-69-6 ]
  • [ 92289-14-0 ]
 

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