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Chemical Structure| 54528-39-1 Chemical Structure| 54528-39-1

Structure of 54528-39-1

Chemical Structure| 54528-39-1

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Product Details of [ 54528-39-1 ]

CAS No. :54528-39-1
Formula : C18H16O5
M.W : 312.32
SMILES Code : O=C1C(C2=CC=C(OC)C(OC)=C2)=C(C)OC3=C1C=CC(O)=C3
MDL No. :MFCD03266962

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Application In Synthesis of [ 54528-39-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54528-39-1 ]

[ 54528-39-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 50-00-0 ]
  • [ 54528-39-1 ]
  • [ 494-52-0 ]
  • 7-hydroxy-3-(3,4-dimethoxyphenyl)-2-methyl-8-[(2S)-2-pyridin-3-ylpiperidin-1-yl]methyl}-4H-chromen-4-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
95% With dmap; In ethanol; at 78℃; General procedure: A solution of 2a-h (2 mmol) in EtOH (anhydrous,30 mL) was refluxed and treated with anabasine (2.5 mmol), paraformaldehyde (90 mg, 3 mmol), and DMAP (2-5 mg).The mixture was refluxed for 20-25 h. The end of the reaction was determined using TLC. The mixture was cooled and diluted with hexane. The resulting precipitate was filtered off, dried, and crystallized from i-PrOH-hexane or purified bycolumn chromatography using EtOAc as eluent.
 

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Technical Information

• Appel Reaction • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Buchwald-Hartwig C-N Bond and C-O Bond Formation Reactions • Chugaev Reaction • Clemmensen Reduction • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Corey-Kim Oxidation • Dess-Martin Oxidation • Fischer Indole Synthesis • Grignard Reaction • Henry Nitroaldol Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Jones Oxidation • Lawesson's Reagent • Leuckart-Wallach Reaction • Martin's Sulfurane Dehydrating Reagent • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Mitsunobu Reaction • Moffatt Oxidation • Nomenclature of Ethers • Oxidation of Alcohols by DMSO • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Alcohols • Preparation of Aldehydes and Ketones • Preparation of Amines • Preparation of Ethers • Prins Reaction • Reactions of Alcohols • Reactions of Aldehydes and Ketones • Reactions of Amines • Reactions of Benzene and Substituted Benzenes • Reactions of Ethers • Reactions with Organometallic Reagents • Reformatsky Reaction • Ritter Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Sharpless Olefin Synthesis • Specialized Acylation Reagents-Ketenes • Stobbe Condensation • Swern Oxidation • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

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