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Chemical Structure| 54537-47-2 Chemical Structure| 54537-47-2

Structure of 54537-47-2

Chemical Structure| 54537-47-2

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Product Details of [ 54537-47-2 ]

CAS No. :54537-47-2
Formula : C5H10BrNO
M.W : 180.04
SMILES Code : CC(Br)C(N(C)C)=O
MDL No. :MFCD00045031

Safety of [ 54537-47-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P264-P270-P301+P312-P330-P501

Application In Synthesis of [ 54537-47-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54537-47-2 ]

[ 54537-47-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 54537-47-2 ]
  • [ 13659-23-9 ]
  • 2-(2-Bromo-5-chlorophenoxy)-N,N-dimethylpropionamide [ No CAS ]
YieldReaction ConditionsOperation in experiment
With potassium carbonate; In 4-methyl-2-pentanone; EXAMPLE 3 2-(2-Bromo-5-chlorophenoxy)-N,N-dimethylpropionamide (Compound no. 11) <strong>[13659-23-9]2-Bromo-5-chlorophenol</strong> (8 g), 2-bromo-N,N-dimethylpropionamide (6.66 g) and anhydrous potassium carbonate (2.6 g) in methyl iso-butyl ketone (100 ml) were refluxed with stirring overnight. The mixture was cooled to 50 and washed with 5% sodium hydroxide (2*20 ml) and then water (2*50 ml). The organic solution was dried and evaporated under reduced pressure to yield a pale red oil, which solidified on cooling. Recrystallisation from 50% aqueous ethanol gave the title compound, m.p. 76-77. Compounds 2, 9, 10 to 13, 17 and 21 were made by a similar procedure.
 

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