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[ CAS No. 5473-15-4 ] {[proInfo.proName]}

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Chemical Structure| 5473-15-4
Chemical Structure| 5473-15-4
Structure of 5473-15-4 * Storage: {[proInfo.prStorage]}
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Product Details of [ 5473-15-4 ]

CAS No. :5473-15-4 MDL No. :MFCD09475503
Formula : C12H13NO4 Boiling Point : -
Linear Structure Formula :C10H9O3CH3CONH InChI Key :-
M.W : 235.24 Pubchem ID :-
Synonyms :

Safety of [ 5473-15-4 ]

Signal Word:Warning Class:
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 UN#:
Hazard Statements:H302-H315-H319 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 5473-15-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 5473-15-4 ]
  • Downstream synthetic route of [ 5473-15-4 ]

[ 5473-15-4 ] Synthesis Path-Upstream   1~3

  • 1
  • [ 5473-15-4 ]
  • [ 36725-28-7 ]
Reference: [1] Journal of Heterocyclic Chemistry, 1988, vol. 25, # 6, p. 1689 - 1695
  • 2
  • [ 5473-15-4 ]
  • [ 20637-09-6 ]
Reference: [1] Journal of Fluorine Chemistry, 1997, vol. 84, # 2, p. 119 - 126
  • 3
  • [ 5473-15-4 ]
  • [ 15118-60-2 ]
YieldReaction ConditionsOperation in experiment
95% With hydrazine hydrate; potassium hydroxide In diethylene glycol for 1.5 h; Reflux 89 g of 3- (4-acetamidophenyl) propionic acid,88 g of potassium hydroxide, 65 ml of 85percent hydrazine hydrate and 450 ml of diethylene glycol were heated to reflux for 1.5 hours,The temperature was raised to 150 ° C to remove excess hydrazine hydrate,And maintain the temperature for 4 hours, cooled to room temperature, add water 400 grams, 6N hydrochloric acid to adjust PH to 6,PH to 5-6 with glacial acetic acid, crystal precipitation, filtration, washing, drying,Get white or almost white crystals 44g. Yield: 95percent
Reference: [1] Patent: CN104447376, 2016, B, . Location in patent: Paragraph 0032-0033; 0043-0044
[2] European Journal of Medicinal Chemistry, 2018, vol. 146, p. 588 - 598
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