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Chemical Structure| 54764-96-4 Chemical Structure| 54764-96-4

Structure of 54764-96-4

Chemical Structure| 54764-96-4

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Product Details of [ 54764-96-4 ]

CAS No. :54764-96-4
Formula : C6H7NO2
M.W : 125.13
SMILES Code : O=CC1=C(OC)C=CN1
MDL No. :MFCD12923762

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 54764-96-4 ]

[ 54764-96-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 54764-96-4 ]
  • [ 99365-48-7 ]
  • [ 275386-72-6 ]
YieldReaction ConditionsOperation in experiment
83% With piperidine; In isopropyl alcohol; at 85℃; for 2h; A mixture of <strong>[99365-48-7]4-bromo-1,3-dihydro-2H-indol-2-one</strong> (100 mg, 0.47 mmol) (prepared according to T. Kosuge et al., Chem. Pharm. Bull. 33(4):1414-1418 (1985)), and excess 3-methoxy-2-pyrrolecarboxyaldehyde (70.8 mg, 0.57 mmol) (prepared according to F. Bellamy, J. Chem. Research (S) (1979) 18-19; J. Chem. Research (M) (1979) 0106-0116) in 1% piperidine in 2-propanol (1 mL) was heated at 85 C for 2 h. Hot water (1 mL) was added. On cooling, the crystallized product was filtered off, washed with aqueous 2-propanol and dried. (Yield 0.13 g, 83%).
 

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