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Chemical Structure| 55636-09-4 Chemical Structure| 55636-09-4

Structure of 55636-09-4

Chemical Structure| 55636-09-4

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Product Details of [ 55636-09-4 ]

CAS No. :55636-09-4
Formula : C9H24Cl2N2O
M.W : 247.21
SMILES Code : C[N+](C)(C)CC(O)C[N+](C)(C)C.[Cl-].[Cl-]
MDL No. :MFCD30145921

Safety of [ 55636-09-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 55636-09-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55636-09-4 ]

[ 55636-09-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 55636-09-4 ]
  • [ 123-47-7 ]
YieldReaction ConditionsOperation in experiment
79% With potassium iodide; In methanol; at 62℃; for 0.5h; (2) Add 100.0 g (0.405 mol) of pure intermediate ammonium chloride, 148 g (0.893 mol, 2.2 eq) of potassium iodide, and 500 g of methanol into a 2L reaction flask, heat up to 62±2 C for reflux reaction for 0.5 h, and remove by filtration while hot The resulting potassium chloride solid was cooled and crystallized from the filtrate.Suction filtration, the filter cake was washed with methanol 100g×2, and vacuum dried at 45C to obtain 130g of white solid (crude proiodide) with a yield of 75%.Take 100 g of crude proproammonium iodide, add 600 g of ethanol, heat up and reflux to dissolve. Activated carbon 5.0g was added, filtered while hot, and the filtrate was cooled and crystallized. After suction filtration, the filter cake was washed with 100 g × 2 of ethanol, and dried under vacuum at 45 C. to obtain 79 g of a white solid (pure ammonium proiodide) with a yield of 79%. The purity was 100% detected by ion chromatography.
 

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