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Chemical Structure| 55661-08-0 Chemical Structure| 55661-08-0

Structure of 55661-08-0

Chemical Structure| 55661-08-0

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Product Details of [ 55661-08-0 ]

CAS No. :55661-08-0
Formula : C9H11ClO3S
M.W : 234.70
SMILES Code : O=S(C1=C(C)C=C(OC)C=C1C)(Cl)=O
MDL No. :MFCD00210327
InChI Key :FARJAHHRGCAAOY-UHFFFAOYSA-N
Pubchem ID :15917496

Safety of [ 55661-08-0 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P260-P280-P303+P361+P353-P301+P330+P331-P304+P340+P310-P305+P351+P338+P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 55661-08-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 55661-08-0 ]

[ 55661-08-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 55661-08-0 ]
  • [ 341988-36-1 ]
  • [ 1239952-64-7 ]
YieldReaction ConditionsOperation in experiment
99% With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25℃; for 12h; General working procedure GWP I-sulfonylation: A solution of the sulfonyl chloride C (1 equiv.) in dichloromethane was added at room temperature to a solution of the amino acid ester A (1.2 equiv.) and diisopropylethylamine (1 to 3 equiv.) in dichloromethane. The reaction mixture was stirred for 12 h at room temperature, then washed 3.x. with a 1N HCl solution, dried over sodium sulfate and concentrated under reduced pressure. Purification by column chromatography (silica; ethyl acetate/-hexane) yielded the desired product.
 

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