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Chemical Structure| 5586-73-2 Chemical Structure| 5586-73-2
Chemical Structure| 5586-73-2

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CAS No.: 5586-73-2

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Product Details of [ 5586-73-2 ]

CAS No. :5586-73-2
Formula : C15H17N
M.W : 211.30
SMILES Code : NCCC(C1=CC=CC=C1)C2=CC=CC=C2
MDL No. :MFCD00008202
InChI Key :KISZTEOELCMZPY-UHFFFAOYSA-N
Pubchem ID :79698

Safety of [ 5586-73-2 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 5586-73-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 5586-73-2 ]

[ 5586-73-2 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 2286-54-6 ]
  • [ 5586-73-2 ]
  • 3
  • [ 558-42-9 ]
  • [ 5586-73-2 ]
  • 1-(3,3-diphenylpropyl)amino-2-methyl-2-propanol [ No CAS ]
  • 4
  • [ 5586-73-2 ]
  • [ 25271-35-6 ]
  • [ 1041193-10-5 ]
YieldReaction ConditionsOperation in experiment
In a 3 necked flask under an atmosphere, of nitrogen, <strong>[25271-35-6]N-methylpiperidine-2-carboxylic acid hydrochloride</strong> (1.79g, 10.0 mmol), HOBt (1.35g, 10 mmol). EDC hydrochloride (1.92g, 10 mmol) and TEA (3.0Og, 30mmol) were dissolved in CH2Cl2 (100 mL, dry) at 0C. After 30 min, diphenylpropylamine (2.11g, 10 mmol) was added. After 1 more hour stirring at 0C, the mixture was allowed to stir at rt overnight. When TLC showed consumption of (nearly) all starting materials, the reaction mixture was quenched with water (150 mL). The layers were separated and the organic layer was washed with NaHCO3 (50 mL, sat.), dried (MgSO4), filtered and concentrated in vacuo to yield a yellow/orange oil (4.12g). This crude oil was purifierd by chromatography (Silica, CH2C12/CH3OH, gradient 0-3%) to yield a colorless oil (2.6g, 7.7 mmol).
  • 5
  • [ 207399-07-3 ]
  • [ 5586-73-2 ]
  • C51H60N3(1+)*I(1-) [ No CAS ]
 

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