Home Cart Sign in  
Chemical Structure| 56364-25-1 Chemical Structure| 56364-25-1

Structure of 56364-25-1

Chemical Structure| 56364-25-1

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 56364-25-1 ]

CAS No. :56364-25-1
Formula : C15H12O4
M.W : 256.25
SMILES Code : O=C1C(C(/C=C/C2=CC=CC=C2)=O)=C(O)C=C(C)O1
MDL No. :N/A

Safety of [ 56364-25-1 ]

Application In Synthesis of [ 56364-25-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 56364-25-1 ]

[ 56364-25-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 56364-25-1 ]
  • [ 538-28-3 ]
  • [ 101094-02-4 ]
  • 6-phenyl-4-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-S-benzylthiopyrimidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
46% With piperidine; In ethanol;Reflux; General procedure: To a suspension of 1 (1.0 mmol) in alcohol (25 ml)was added SBT (1.0 mmol) with 6-8 drops of piperidine and the solution was refluxed for 3-4 hrs on water bath. Initially, all the reactants dissolved and then a crystalline product separated out. The reaction mixture was allowed to cool to room temperature and the solid product was filtered and washed with alcohol (5-10 ml) to give pure product 3. All the pyrimidine derivatives 3a-j were recrystallized with alcohol. The physical, analytical and spectral data of compounds 3a-j are given. 6-Phenyl-4-(4-hydroxy-6-methyl-2-oxo-2H-pyran-3-yl)-2-S-benzylthiopyrimidine (3a)Yield: 46%; mp 145-46 C; IR (max in KBR): 1703 cm-1(C= O str.); 1H NMR (CDCl3, 300 MHz, ): 2.32 (s, 3H, CH3),4.59 (s, 2H, CH2), 6.02 (s, 1H, =CH), 7.30-8.08 (m, 10H, Ar),8.9 (s, 1H, C5-H of pyrimidine). Mass (m/z): 402, ElementalAnalysis: C23H18N2O3S found: C, 68.68; H, 4.50; N, 6.92,requires: C, 68.64; H, 4.51; N, 6.96.
 

Historical Records

Technical Information

Categories