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[ CAS No. 57273-36-6 ]

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Chemical Structure| 57273-36-6
Chemical Structure| 57273-36-6
Structure of 57273-36-6 * Storage: {[proInfo.prStorage]}

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Product Details of [ 57273-36-6 ]

CAS No. :57273-36-6 MDL No. :MFCD07783396
Formula : C5H3NaO3 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :134.07 g/mol Pubchem ID :-
Synonyms :

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Application In Synthesis of [ 57273-36-6 ]

  • Downstream synthetic route of [ 57273-36-6 ]

[ 57273-36-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1271-19-8 ]
  • [ 57273-36-6 ]
  • bis(η5-cyclopentadienyl)bis(furan-2-carboxylato-κO)titanium(IV) [ No CAS ]
YieldReaction ConditionsOperation in experiment
65% In benzene; at 40℃; for 4h; A freshly prepared solution of titanocene dichloride (0.25 g, 1.004 mmol) in anhydrousbenzene (15 mL) was added to a stirred suspension of sodium 4-methylbenzoate(0.396 g, 2.504 mmol) in anhydrous benzene (15 mL) and the stirring was continuedat 40 C for 4 h. During reaction, the color of the reaction mixture changed from blood-red to bright-orange. The orange solution was filtered through a frit coveredwith pre-dried neutral silica (1 cm layer, mesh size 100-200) and eluted further withanhydrous benzene (30.5 mL). The clear filtrate was concentrated using a rotaryevaporator to around 5mL and precipitated with excess anhydrous hexane. Theorange solid was collected on a frit, washed with hexane (25 mL), dried, and recrystallizedfrom anhydrous toluene under ambient conditions to afford orange crystals of1 at ambient temperature.
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