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Chemical Structure| 57641-89-1 Chemical Structure| 57641-89-1

Structure of 57641-89-1

Chemical Structure| 57641-89-1

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Product Details of [ 57641-89-1 ]

CAS No. :57641-89-1
Formula : C9H14O2
M.W : 154.21
SMILES Code : CCCC1CC(=O)CC(=O)C1
MDL No. :MFCD00129456

Safety of [ 57641-89-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 57641-89-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 57641-89-1 ]

[ 57641-89-1 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 178686-24-3 ]
  • [ 1118-61-2 ]
  • [ 57641-89-1 ]
  • 4-(3-ethoxy-4-hydroxy-5-nitro-phenyl)-2-methyl-5-oxo-7-propyl-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; for 17.0h;Heating / reflux; (b). 4-(3-Ethoxy-4-hvdroxy-5-nitro-phenviy2-methyl-5-oxo-7-propyl-l,4,5, 6,7,8- hexahydro-quinoline-3 -carbonitrileA mixture of <strong>[178686-24-3]3-ethoxy-4-hydroxy-5-nitro-benzaldehyde</strong> (1.5 g), 3-aminocrotonitrile (584 mg) and 5-propylcyclohexane-l,3-dione (1.09 g) in ethanol (60 ml) was heated at reflux for 17 h. The mixture was concentrated in vacuo. The residue was purified by chromatography on silicagel in heptane/ethyl acetate 1/0 - > 0/1 (v/v) as eluent. EPO <DP n="43"/>Yield: 1.3 g. MS-ESI: [M+H]+ = 412.3
  • 2
  • [ 178686-24-3 ]
  • [ 870-64-4 ]
  • [ 57641-89-1 ]
  • 4-(3-ethoxy-4-hydroxy-5-nitro-phenyl)-2-methyl-5-oxo-7-propyl-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile [ No CAS ]
YieldReaction ConditionsOperation in experiment
In ethanol; for 17.0h;Heating / reflux; (b). 4-(3-Ethoxy-4-hydroxy-5-nitro-phenyl)-2-methyl-5-oxo-7-propyl-1,4,5,6,7,8-hexahydro-quinoline-3-carbonitrile A mixture of <strong>[178686-24-3]3-ethoxy-4-hydroxy-5-nitro-benzaldehyde</strong> (1.5 g), 3-aminocrotonitrile (584 mg) and 5-propylcyclohexane-1,3-dione (1.09 g) in ethanol (60 ml) was heated at reflux for 17 h. The mixture was concentrated in vacuo. The residue was purified by chromatography on silicagel in heptane/ethyl acetate 1/0?0/1 (v/v) as eluent.Yield: 1.3 g. MS-ESI: [M+H]+=412.3
 

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