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Chemical Structure| 578703-90-9 Chemical Structure| 578703-90-9

Structure of 578703-90-9

Chemical Structure| 578703-90-9

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Product Details of [ 578703-90-9 ]

CAS No. :578703-90-9
Formula : C9H6FN3O
M.W : 191.16
SMILES Code : O=CC1=CN(C2=CC=C(F)C=C2)N=N1
MDL No. :MFCD10696362

Safety of [ 578703-90-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P312-P362-P403+P233-P501

Application In Synthesis of [ 578703-90-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 578703-90-9 ]

[ 578703-90-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 57497-39-9 ]
  • [ 578703-90-9 ]
  • [ 1613039-82-9 ]
YieldReaction ConditionsOperation in experiment
85% With sodium hydrogencarbonate; In ethanol; at 60℃; General procedure: A mixture of 1-substituted-1H-1,2,3-triazole-4-carbaldehyde 2 (1mmol), N-benzyl/t-butyl hydroxylamine hydrochloride (1.5mmol) and sodium bicarbonate (1.5mmol) in absolute ethanol (6mL) was heated at 60C until the carbonyl compound was disappeared (monitored by TLC). The solvent was removed in vacuo and the reaction mixture was diluted with H2O and extracted with EtOAc. Combined organic layers dried over anhydrous sodium sulfate and concentrated. The residue was purified by column chromatography (SiO2, mixtures of petroleum ether/EtOAc).
 

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