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[ CAS No. 58621-39-9 ] {[proInfo.proName]}

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Chemical Structure| 58621-39-9
Chemical Structure| 58621-39-9
Structure of 58621-39-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 58621-39-9 ]

CAS No. :58621-39-9 MDL No. :
Formula : C11H12O2 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 176.21 Pubchem ID :-
Synonyms :

Safety of [ 58621-39-9 ]

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Application In Synthesis of [ 58621-39-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 58621-39-9 ]

[ 58621-39-9 ] Synthesis Path-Downstream   1~16

  • 1
  • [ 58621-39-9 ]
  • [ 2150-42-7 ]
  • [ 198351-02-9 ]
  • 2
  • [ 58621-39-9 ]
  • [ 20029-76-9 ]
  • [ 198351-11-0 ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid; sodium hydride 1) THF, reflux, 5 h, 2) THF, MeOH, reflux, 3 h; Yield given. Multistep reaction;
  • 3
  • [ 58621-39-9 ]
  • [ 78955-90-5 ]
  • [ 198351-08-5 ]
  • 4
  • [ 13129-23-2 ]
  • [ 58621-39-9 ]
  • 8-Allyl-2-furan-3-yl-chromen-4-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid; sodium hydride 1) THF, reflux, 5 h, 2) THF, MeOH, reflux, 3 h; Multistep reaction;
  • 5
  • [ 22913-26-4 ]
  • [ 58621-39-9 ]
  • [ 219771-87-6 ]
  • 6
  • [ 81452-54-2 ]
  • [ 58621-39-9 ]
  • [ 219771-88-7 ]
  • 7
  • [ 5118-06-9 ]
  • [ 58621-39-9 ]
  • 8-Allyl-2-(3-hydroxy-thiophen-2-yl)-chromen-4-one [ No CAS ]
  • 8
  • [ 35475-03-7 ]
  • [ 58621-39-9 ]
  • [ 219771-97-8 ]
  • 9
  • [ 62224-16-2 ]
  • [ 58621-39-9 ]
  • [ 219771-99-0 ]
  • 10
  • [ 78071-37-1 ]
  • [ 58621-39-9 ]
  • [ 219771-94-5 ]
  • 11
  • [ 62353-75-7 ]
  • [ 58621-39-9 ]
  • [ 219771-89-8 ]
YieldReaction ConditionsOperation in experiment
With sulfuric acid; sodium hydride 1) THF, reflux, 5 h, 2) THF, MeOH, reflux, 3 h; Yield given. Multistep reaction;
  • 12
  • [ 58621-39-9 ]
  • [ 88770-19-8 ]
  • [ 219771-93-4 ]
  • 13
  • [ 58621-39-9 ]
  • [ 76360-42-4 ]
  • [ 219771-95-6 ]
  • 14
  • [ 58621-39-9 ]
  • [ 4460-86-0 ]
  • 1-(2-hydroxy-3-allyl-phenyl)-3-(2,4,5-trimethoxy-phenyl)-propenone [ No CAS ]
YieldReaction ConditionsOperation in experiment
100% With potassium hydroxide In ethanol for 191h; 15 [1-(2-HYDROXY-3-ALLYL-PHENYL)-3-(2,] 4, [5-TRIMETHOXY-] phenyl)-propenone (74) To a stirring suspension of [1- (3-ALLYL-2-HYDROXY-] phenyl)-ethanone 73 (1.779 g, 27 mmol) and 2,4, 5- trimethoxy benzaldehyde (5.89 g, 30 mmol, 1.1 equ) in ethanol (50 ml) was added potassium hydroxide (3.23 g, 58 mmol, 2.1 equ). The reaction mixture was stirred for [191] hours then acidified (2 M [HC1)] and extracted with ethyl acetate (3x). The combined organic layers were then washed with water and brine then dried (MgSO4) and concentrated in vacuo to give [1- (2-HYDROXY-3-ALLYL-PHENYL)-3- (2,] 4,5- trimethoxy-phenyl)-propenone 74 (11.165 g, 116 %) as an orange solid. [H] nmr (400 MHz, CDCl3) 3.47 (d, 2H, 6.6 Hz) 3.92 (s, 3H) 3.94 (s, 3H) 3.96 (s, 3H) 5.08-5. 14 (m, 2H) 5.99-6. 10 (m, 1H) 6.53 (s, 1H) 6.88 (t, 1H, 7.7 Hz) 7.13 (s, 1H) 7.36 (d, 1H, 6.5 Hz) 7.63 (d, 1H, 15.5 Hz) 7.82 (dd, 1H, 1.4+8. 1 Hz) 8.21 (d, 1H, 15.5 Hz) 13.43 (s, [1H). 13C] nmr (100 MHz, CDCl3) 33.94 (CH2) 56.49 (CH3) 56.73 [(CH3)] 57.08 (CH3) 97.12 (CH) 112.20 (CH) 115.69 (Q) 116.31 [(CH2)] 118.49 (CH) 118.57 (CH) 120.19 (Q) 128.04 (CH) 129.80 (Q) 136.29 (CH) 136.68 (CH) 138.51 (Q) 141.12 (CH) 143.71 (Q) 153.33 [(Q)] 155.46 (CH) 161.97 (Q) 194.66 (Q). EI+ 354.4 [(69%,] [M+)] 323.3 [(100W,] [[M-OME] +)] [C21H2205] Calc. 354.1467 Found 354.1468.
With potassium hydroxide In ethanol for 191h;
  • 15
  • [ 58621-39-9 ]
  • [ 67127-78-0 ]
  • 16
  • [ 58621-39-9 ]
  • [ 23343-06-8 ]
  • β-(2'-allyloxy-3'-methoxyphenyl)-1-(3-allyl-2-hydroxyphenyl)propenone [ No CAS ]
YieldReaction ConditionsOperation in experiment
74% With potassium hydroxide In ethanol at 0℃; for 24h;
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