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Chemical Structure| 606091-78-5 Chemical Structure| 606091-78-5

Structure of 606091-78-5

Chemical Structure| 606091-78-5

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Product Details of [ 606091-78-5 ]

CAS No. :606091-78-5
Formula : C9H6N4OS
M.W : 218.24
SMILES Code : S=C1OC(C2=CC=C3N=CNC3=C2)=NN1

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Application In Synthesis of [ 606091-78-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 606091-78-5 ]

[ 606091-78-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 606091-78-5 ]
  • [ 4761-00-6 ]
  • [ 1030839-09-8 ]
YieldReaction ConditionsOperation in experiment
63% With triethylamine; In ethanol;Heating / reflux; 5-(5-(2,4,6 Trimethylbenzylthio)-1 ,3,4-oxadiazol-2-yl)-1 H-benzo[d]imidazole 1 (0.33 g, 1.5 mmol), TEA (0.209 mL, 1.5mmol) and 2,4,6-Trimethylbenzylbromide (0.253 g, 1.5 mmol) were dissolved in 10 mL of EtOH and kept under reflux overnight. The solvent was removed and the remaining oil was purified by flash-chromatography on silica gel, applying aCHCIs/MeOH gradient.Yield: 0.332 g (63%), MS: m/z 351.3 [M+H]+, HPLC (214 nm): rt 12.37 min (89.8%)
 

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