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Chemical Structure| 60770-51-6 Chemical Structure| 60770-51-6

Structure of 60770-51-6

Chemical Structure| 60770-51-6

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Product Details of [ 60770-51-6 ]

CAS No. :60770-51-6
Formula : C8H5IO2
M.W : 260.03
SMILES Code : O=C1COC2=CC=C(I)C=C12
MDL No. :MFCD12187642

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Application In Synthesis of [ 60770-51-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 60770-51-6 ]

[ 60770-51-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 60770-51-6 ]
  • [ 33906-30-8 ]
  • 2-[<i>N</i>'-(5-iodo-benzofuran-3-ylidene)-hydrazino]-benzoic acid [ No CAS ]
  • 2
  • [ 60770-51-6 ]
  • [ 33906-30-8 ]
  • o-[(2,3-dihydro-5-iodobenzofuran-3-ylidene)hydrazino]-benzoic acid [ No CAS ]
YieldReaction ConditionsOperation in experiment
0.480 g (58%) In ethanol; water; Step 1) Preparation of o-[(2,3-dihydro-5-iodobenzofuran-3-ylidene)hydrazino]-benzoic acid To a solution of 5-iodo-3(2H)-benzofuranone (0.551 g, 2.12 mmol) [Cagniant, P. et al. Hebd. Seances Acad. Sci., Ser. C, 1976, 282 (21), 993-6] in ethanol (100 mL) was added a solution of <strong>[33906-30-8]2-hydrazinobenzoic acid hydrochloride</strong> (0.800 g, 4.24 mmol) in deionized water (50 mL). The mixture was stirred for one hour at room temperature and then allowed to sit while cooled (0 C.). Vacuum filtration and drying in vacuo afforded 0.480 g (58%) of the title compound as a tan solid: mp 169 C.(dec) which was used without further purification.
 

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