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[ CAS No. 613-12-7 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
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Chemical Structure| 613-12-7
Chemical Structure| 613-12-7
Structure of 613-12-7 * Storage: {[proInfo.prStorage]}
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Product Details of [ 613-12-7 ]

CAS No. :613-12-7 MDL No. :MFCD00003583
Formula : C15H12 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 192.26 Pubchem ID :-
Synonyms :

Safety of [ 613-12-7 ]

Signal Word:Danger Class:9
Precautionary Statements:P201-P264-P280-P301+P330+P331-P312 UN#:3077
Hazard Statements:H302-H361-H372-H410 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 613-12-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 613-12-7 ]

[ 613-12-7 ] Synthesis Path-Downstream   1~14

  • 3
  • [ 613-12-7 ]
  • [ 177839-45-1 ]
YieldReaction ConditionsOperation in experiment
90% With N-Bromosuccinimide; trifluoroacetic acid; In chloroform; at 20℃;Inert atmosphere; Schlenk technique; To a 250mL round bottom flask, the compound MA (1.00g, 5.20mmol), n-bromosuccinimide (NBS) (2.23g, 12.00mmol) and 200μL trifluoroacetic acid was dissolved in 20mL chloroform. The solution was stirred overnight at room temperature. After reaction, most of chloroform was evaporated, methanol was then added, a yellow needle-like crystal was obtained (90% yield). 1H NMR (400MHz, CDCl3): δ (ppm) 8.58-8.54 (m, 2H), 8.48 (d, J=9.22Hz, 1H), 8.34 (s, 1H), 7.64-7.58 (m, 2H), 7.46 (dd, J1=1.52Hz, J2=8.96Hz, 1H), 2.63 (d, J=0.72Hz, 3H). 13C NMR (100MHz, CDCl3): δ (ppm) 137.39, 131.04, 130.99, 130.40, 130.11, 129.61, 128.17, 128.07, 128.03, 127.22, 126.89, 126.34, 123.32, 122.34, 22.04. MS (MALDI-TOF) m/z=349.9127 (M+)
  • 4
  • [ 84-54-8 ]
  • [ 613-12-7 ]
YieldReaction ConditionsOperation in experiment
78% With copper(ll) sulfate pentahydrate; ammonia; zinc; In water; at 85℃;Inert atmosphere; Schlenk technique; To a 250mL round bottom flask, MAq (4.00g, 18.00mmol), zinc powder (3.50g, 72.00mmol), cupric sulfate pentahydrate (0.10g, 0.40mmol) and ammonia solution (200.00g) were added. The mixture was heated to 85C and it turned from red to colorless. After filtration, the residue was washed by acetone. The acetone was then evaporated and methanol was added, a white solid was precipitated by adding conc. HCl (87% yield). 1H NMR (400MHz, CDCl3): delta (ppm) 8.37 (s, 1H), 8.31 (s, 1H), 7.99-7.96 (m, 2H), 7.91 (d, J=8.68Hz, 1H), 7.75 (s, 1H), 7.45-7.40 (m, 2H), 7.31 (dd, J1=1.60Hz, J2=8.68Hz, 1H), 2.55 (d, J=0.40Hz, 3H). 13C NMR (100MHz, CDCl3): delta (ppm) 134.88, 131.95, 131.80, 131.18, 130.29, 128.22, 128.15, 128.03, 127.93, 126.29, 125.91, 125.20, 125.13, 124.88, 21.98. MS (MALDI-TOF) m/z=193.1024 (M+H).
  • 5
  • [ 65232-41-9 ]
  • [ 613-12-7 ]
  • [ 2571-52-0 ]
  • [ 610-46-8 ]
  • [ 73466-76-9 ]
  • [ 100-47-0 ]
  • 6
  • [ 5467-99-2 ]
  • [ 120-12-7 ]
  • [ 620-47-3 ]
  • [ 613-12-7 ]
YieldReaction ConditionsOperation in experiment
1: 20% 2: 13% 3: 30% at 400℃;
  • 7
  • [ 605-48-1 ]
  • [ 613-12-7 ]
  • [ 177552-87-3 ]
YieldReaction ConditionsOperation in experiment
10% In dichloromethane Irradiation;
  • 8
  • polyethylene [ No CAS ]
  • [ 612-94-2 ]
  • [ 883-20-5 ]
  • [ 2444-68-0 ]
  • [ 613-12-7 ]
  • 10
  • [ 613-12-7 ]
  • [ 7732-18-5 ]
  • [ 7697-37-2 ]
  • [ 117-78-2 ]
  • 11
  • [ 613-12-7 ]
  • [ 64-19-7 ]
  • chromic acid [ No CAS ]
  • [ 84-54-8 ]
  • [ 117-78-2 ]
  • 12
  • [ 60288-22-4 ]
  • [ 613-12-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: zinc; acetic acid 2: benzene / Kochen des Reaktionsprodukts mit Chromessigsaeure
  • 13
  • [ 613-08-1 ]
  • [ 613-12-7 ]
  • 14
  • [ 120-12-7 ]
  • [ 91-20-3 ]
  • [ 612-00-0 ]
  • [ 106-42-3 ]
  • [ 643-58-3 ]
  • [ 2141-42-6 ]
  • [ 613-12-7 ]
  • [ 108-88-3 ]
  • [ 91-57-6 ]
YieldReaction ConditionsOperation in experiment
1: 0.51 %Chromat. 2: 0.28 %Chromat. 3: 19.84 %Chromat. 4: 4.5 %Chromat. 5: 16.82 %Chromat. 6: 9.79 %Chromat. 7: 6.8 %Chromat. 8: 6.09 %Chromat. With nickel(II) oxide; carbon monoxide; water at 400℃; for 1h; Inert atmosphere; Pyrolysis; 2.2. Hydrogenation experiments of anthracene via the WGSR General procedure: The hydrogenation processes were performed in a 60 mL automaticmagnetic stirring reactor. There, 5.0 g of anthracene, a NiO catalyst(prescribed Ni atomic/anthracene mass ratio of 6%), and 2.0 g ofdeionized water or heavy water (prescribed water/anthracene ratio of0.4), were periodically charged into the reactor. For each run, thereactor was charged with deionized water/heavy water, anthracene, andNiO. Subsequently, the reactor was sealed and purged with N2 six times,and CO was repeatedly filled and discharged three times to ensure thepurity of the gas in the reactor. After the gas was purified by CO, thereactor was pressurized to 4 MPa and heated to the required temperature(400 °C) according to the established procedure. During the heatingprocess, the reactants were fully stirred by the automatic magneticstirring reactor impeller at the speed of 300 rpm to ensure the uniformityof materials and catalysts in the system. After the reaction had beenmaintained for 60 min, the reactor was quickly quenched to 25 °C withcool water.
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