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Chemical Structure| 620-80-4 Chemical Structure| 620-80-4

Structure of 620-80-4

Chemical Structure| 620-80-4

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Product Details of [ 620-80-4 ]

CAS No. :620-80-4
Formula : C13H14O3
M.W : 218.25
SMILES Code : CC(/C(C(OCC)=O)=C\C1=CC=CC=C1)=O
MDL No. :MFCD00521137
InChI Key :AYZGINZXVVKWKV-FMIVXFBMSA-N
Pubchem ID :5376216

Safety of [ 620-80-4 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 620-80-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 620-80-4 ]

[ 620-80-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2725-60-2 ]
  • [ 620-80-4 ]
  • [ 6963-62-8 ]
YieldReaction ConditionsOperation in experiment
70% With ethanol; sodium ethanolate; for 1.5h; General procedure: To a stirred solution of 7 (0.5mmol, 1 equiv) and alpha-diazo-beta-ketosulfone 2 (143mg, 0.6mmol, 1.2 equiv) in dry EtOH (5mL) was added NaOEt (51mg, 0.75mmol, 1.5 equiv) at 0C and the resulting mixture was stirred at the same temperature until the reaction was complete (monitored by TLC). Then the reaction mixture was concentrated in vacuo and the crude residue was directly subjected to silica gel column chromatography (pet ether/ethyl acetate: 8/2) to afford pure 3, 5 or 8.
 

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