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[ CAS No. 62147-49-3 ] {[proInfo.proName]}

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Chemical Structure| 62147-49-3
Chemical Structure| 62147-49-3
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Product Details of [ 62147-49-3 ]

CAS No. :62147-49-3 MDL No. :MFCD00051019
Formula : C6H12O6 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 180.16 Pubchem ID :-
Synonyms :

Safety of [ 62147-49-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P301+P312-P302+P352-P304+P340-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 62147-49-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 62147-49-3 ]
  • Downstream synthetic route of [ 62147-49-3 ]

[ 62147-49-3 ] Synthesis Path-Upstream   1~17

  • 1
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Reference: [1] Patent: WO2014/138666, 2014, A1, . Location in patent: Paragraph 0042-0044
  • 2
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Reference: [1] Patent: WO2014/138666, 2014, A1, . Location in patent: Paragraph 0042-0044
  • 3
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Reference: [1] Angewandte Chemie - International Edition, 2010, vol. 49, # 49, p. 9456 - 9459
  • 4
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  • [ 40031-31-0 ]
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 5
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 6
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 7
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 8
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 9
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 10
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Reference: [1] RSC Advances, 2015, vol. 5, # 110, p. 90952 - 90959
  • 11
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  • [ 64-18-6 ]
  • [ 10326-41-7 ]
Reference: [1] RSC Advances, 2015, vol. 5, # 110, p. 90952 - 90959
  • 12
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  • [ 78-98-8 ]
Reference: [1] RSC Advances, 2015, vol. 5, # 110, p. 90952 - 90959
  • 13
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Reference: [1] Carbohydrate Research, 1983, vol. 116, p. 197 - 208
  • 14
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  • [ 38993-84-9 ]
Reference: [1] Patent: US6511978, 2003, B1,
  • 15
  • [ 62147-49-3 ]
  • [ 593-51-1 ]
  • [ 333-20-0 ]
  • [ 38993-84-9 ]
Reference: [1] Organic and Biomolecular Chemistry, 2007, vol. 5, # 20, p. 3299 - 3309
  • 16
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  • [ 534-03-2 ]
  • [ 78531-52-9 ]
Reference: [1] Journal of Organic Chemistry, 2010, vol. 75, # 13, p. 4472 - 4479
  • 17
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  • [ 10318-18-0 ]
  • [ 73978-41-3 ]
YieldReaction ConditionsOperation in experiment
45% With ammonium chloride In water A.
2,4-Diamino-6-(hydroxymethyl)-pteridine hydrochloride
To a solution of 42.8 g (0.167 mol) of 2,4,5,6-tetraminopyrimidine sulfate monohydrate, which had been recrystallized from boiling 1N sulfuric acid, in 700 ml of boiling water was added gradually a solution of 40.7 g (0.167 mol) of barium chloride dihydrate in 100 ml water.
After a short period of digestion, the mixture was filtered from the precipitated barium sulfate, the filtrate was stirred with 5 g of decolorizing carbon and filtered again.
This solution was added to a stirred mixture of 426 g of ammonium chloride, 26.3 g (0.167 mol) of cysteine hydrochloride, 46.6 g (0.259 mol) of dihydroxyacetone dimer and 970 mol of water in a 3-l three-necked flask equipped with a stirrer and a glass-fitted gas inlet tube.
The resulting mixture was stirred for 67 hours at room temperature during which time a slow stream of oxygen was passed through the mixture via the gas inlet tube.
The product, 2,4-diamino-6-(hydroxymethyl)-pteridine hydrochloride, separates as a tan solid which was collected by suction filtration, washed with water, and air dried; yield, 17.2 g (45percent).
Reference: [1] Patent: US4820706, 1989, A,
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