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Chemical Structure| 625122-36-3 Chemical Structure| 625122-36-3

Structure of 625122-36-3

Chemical Structure| 625122-36-3

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Product Details of [ 625122-36-3 ]

CAS No. :625122-36-3
Formula : C13H19ClO2
M.W : 242.74
SMILES Code : O=C(OC1(C)C(C2)CC3CC2CC1C3)CCl
MDL No. :N/A

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Application In Synthesis of [ 625122-36-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 625122-36-3 ]

[ 625122-36-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 625122-36-3 ]
  • [ 652-34-6 ]
  • C20H20F4O5 [ No CAS ]
YieldReaction ConditionsOperation in experiment
2.31 parts of the compound represented by the formula (I-1-a), 10 parts of dimethylformamide and carbonic acidAfter mixing 0.80 parts of potassium and stirring at 23 C for 30 minutes, the mixture was further stirred at 80 C for 1 hour.I stirred. The obtained mixed solution was added with 2.93 parts of a compound represented by the formula (I-211-b) and a yolk.Add 0.05 parts of potassium iodide,After stirring at 80 C for 6 hours, the mixture was cooled to 23 C.20 parts of chloroform and 10 parts of ion-exchanged water were added to the obtained reaction mixture, and the mixture was heated at 23 C. for 30 minutes.After stirring for a while, the layers were separated and the organic layer was taken out. To the obtained organic layer, 10 parts of ion-exchanged water was added, and the mixture was stirred at 23 C. for 30 minutes, then liquid-separated, and the organic layer was taken out. This water washing operation was repeated 3 times. The obtained organic layer was concentrated, and the concentrated mixture was subjected to a column (silica gel 60N (spherical, neutral) 100-210 μm; manufactured by Kanto Chemical Co., Inc., developing solvent: n-heptane / ethyl acetate = 1/1). By collecting3.92 parts of the compound represented by the formula (I-211-c) was obtained.
 

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