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Chemical Structure| 62532-99-4 Chemical Structure| 62532-99-4

Structure of 62532-99-4

Chemical Structure| 62532-99-4

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Product Details of [ 62532-99-4 ]

CAS No. :62532-99-4
Formula : C10H9NS
M.W : 175.25
SMILES Code : NC1=CC=CC=C1C2=CC=CS2
MDL No. :MFCD04039147

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Application In Synthesis of [ 62532-99-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 62532-99-4 ]

[ 62532-99-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 62532-99-4 ]
  • [ 110677-45-7 ]
  • C29H18N2S [ No CAS ]
YieldReaction ConditionsOperation in experiment
54% With trifluoroacetic acid; In toluene; at 130℃; for 72h; 2-(2-thienyl)aniline (5.3 g, 30 mmol), 4-(carbazol-9-yl)carbaldehyde (11.9 g, 50 mmol), 10 mL of trifluoroacetic acid and 100 mL of toluene were added to a 250 mL round bottom flask. The mixture was heated and stirred at 130C for three days. Cool to room temperature, quench with aqueous sodium hydroxide, extract with dichloromethane, and remove the solvent on a rotary evaporator. Purification by column chromatography. A white solid (13.5 g, 54%) was obtained.
  • 2
  • [ 66-39-7 ]
  • [ 62532-99-4 ]
  • C23H15NO2S2 [ No CAS ]
YieldReaction ConditionsOperation in experiment
57% With trifluoroacetic acid; In toluene; at 130℃; for 72h; 2-(2-thienyl)aniline (5.3 g, 30 mmol), diphenylthiophenol (11.5 g, 50 mmol), 10 mL of trifluoroacetic acid and 100 mL of toluene, and the mixture was stirred at 130C for three days with heating. Cool to room temperature, quench with aqueous sodium hydroxide, extract with dichloromethane, and remove the solvent on a rotary evaporator. Purification by column chromatography. A white solid (12.6 g, 57%) was obtained.
 

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