[ CAS No. 6323-18-8 ] {[proInfo.proName]}

Name: 6323-18-8|1-(2-Chlorophenyl)propan-1-one|95%
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Quality Control of [ 6323-18-8 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification

Alternatived Products of [ 6323-18-8 ]

Product Details of [ 6323-18-8 ]

CAS No. :	6323-18-8	MDL No. :	MFCD07787256
Formula :	C₉H₉ClO	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	BTSCBJDORATYKJ-UHFFFAOYSA-N
M.W :	168.62	Pubchem ID :	95743
Synonyms :

Safety of [ 6323-18-8 ]

Signal Word:	Warning	Class:	N/A
Precautionary Statements:	P261-P305+P351+P338	UN#:	N/A
Hazard Statements:	H302-H315-H319-H335	Packing Group:	N/A
GHS Pictogram:

Application In Synthesis of [ 6323-18-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Upstream synthesis route of [ 6323-18-8 ]
Downstream synthetic route of [ 6323-18-8 ]

[ 6323-18-8 ] Synthesis Path-Upstream 1~11

1
[ 6323-18-8 ]
[ 6305-95-9 ]

Reference： [1] Tetrahedron Letters, 1977, p. 2639 - 2642

2
[ 22869-35-8 ]
[ 6323-18-8 ]

Reference： [1] Tetrahedron, 2007, vol. 63, # 12, p. 2695 - 2711
[2] European Journal of Medicinal Chemistry, 1995, vol. 30, # 1, p. 85 - 94
[3] Journal of Organic Chemistry, 2003, vol. 68, # 4, p. 1594 - 1596

3
[ 873-32-5 ]
[ 925-90-6 ]
[ 6323-18-8 ]

Reference： [1] Tetrahedron Letters, 2007, vol. 48, # 42, p. 7448 - 7451
[2] Chemistry - A European Journal, 2005, vol. 11, # 23, p. 6889 - 6904

4
[ 1196-28-7 ]
[ 6323-18-8 ]

Reference： [1] Journal of Organic Chemistry, 1946, vol. 11, p. 444,447

5
[ 873-32-5 ]
[ 6323-18-8 ]
[ 75815-22-4 ]

Reference： [1] Patent: US4690931, 1987, A,

6
[ 89-98-5 ]
[ 6323-18-8 ]

Reference： [1] Tetrahedron, 2007, vol. 63, # 12, p. 2695 - 2711

7
[ 10467-10-4 ]
[ 873-32-5 ]
[ 6323-18-8 ]

Reference： [1] Tetrahedron, 1978, vol. 34, p. 1627 - 1631

8
[ 609-02-9 ]
[ 609-65-4 ]
[ 6323-18-8 ]

Reference： [1] Journal fuer Praktische Chemie (Leipzig), 1963, vol. 22, p. 202 - 213

9
[ 6323-18-8 ]
[ 75815-22-4 ]

Reference： [1] Journal fuer Praktische Chemie (Leipzig), 1963, vol. 22, p. 202 - 213
[2] Journal of Organic Chemistry, 2003, vol. 68, # 4, p. 1594 - 1596
[3] MedChemComm, 2016, vol. 7, # 7, p. 1441 - 1448

10
[ 873-32-5 ]
[ 6323-18-8 ]
[ 75815-22-4 ]

Reference： [1] Patent: US4690931, 1987, A,

11
[ 6323-18-8 ]
[ 18776-12-0 ]

Reference： [1] Patent: EP591584, 1994, A1,

[ 6323-18-8 ] Synthesis Path-Downstream 1~62

1
[ 1196-28-7 ]
[ 6323-18-8 ]

Reference： [1]Journal of Organic Chemistry,1946,vol. 11,p. 444,447

2
[ 6323-18-8 ]
[ 6305-95-9 ]

Reference： [1]Tetrahedron Letters,1977,p. 2639 - 2642

3
[ 6323-18-8 ]
[ 35996-45-3 ]

Reference： [1]Journal of Organic Chemistry,1973,vol. 38,p. 835 - 838
[2]Tetrahedron,1978,vol. 34,p. 1627 - 1631

4
[ 42596-46-3 ]
[ 6323-18-8 ]
[ 122433-05-0 ]

Reference： [1]European Journal of Medicinal Chemistry,1990,vol. 25,p. 785 - 788

5
[ 6323-18-8 ]
[ 22869-35-8 ]

Reference： [1]Synthesis,1982,p. 732 - 735

6
[ 6323-18-8 ]
[ 81671-55-8 ]

Reference： [1]Journal of Organic Chemistry,1982,vol. 47,p. 2795 - 2798

7
[ 6323-18-8 ]
(R)-1-(2-chlorophenyl)propanol [ No CAS ]
[ 158635-38-2 ]

Reference： [1]Journal of the American Chemical Society,1993,vol. 115,p. 9800 - 9801
[2]Chirality,2010,vol. 22,p. 173 - 181

8
[ 50-00-0 ]
[ 6323-18-8 ]
[ 25150-61-2 ]
1-(2-Chloro-phenyl)-2-methyl-3-pyrrolidin-1-yl-propan-1-one [ No CAS ]

Reference： [1]European Journal of Medicinal Chemistry,1995,vol. 30,p. 85 - 94

9
[ 22869-35-8 ]
[ 6323-18-8 ]

Reference： [1]Tetrahedron,2007,vol. 63,p. 2695 - 2711
[2]European Journal of Medicinal Chemistry,1995,vol. 30,p. 85 - 94
[3]Journal of Organic Chemistry,2003,vol. 68,p. 1594 - 1596

10
[ 10467-10-4 ]
[ 873-32-5 ]
[ 6323-18-8 ]

Reference： [1]Tetrahedron,1978,vol. 34,p. 1627 - 1631

11
[ 6323-18-8 ]
[ 69086-88-0 ]

Reference： [1]Tetrahedron,1978,vol. 34,p. 1627 - 1631

12
[ 6323-18-8 ]
[ 75815-22-4 ]

Reference： [1]Journal fur praktische Chemie (Leipzig 1954),1963,vol. 22,p. 202 - 213
[2]Journal of Organic Chemistry,2003,vol. 68,p. 1594 - 1596
[3]MedChemComm,2016,vol. 7,p. 1441 - 1448

13
[ 609-02-9 ]
[ 609-65-4 ]
[ 6323-18-8 ]

Reference： [1]Journal fur praktische Chemie (Leipzig 1954),1963,vol. 22,p. 202 - 213

15
[ 6323-18-8 ]
1-(2-chloro-phenyl)-propan-1-one oxime [ No CAS ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

16
[ 6323-18-8 ]
[ 616-34-2 ]
[1-(2-chloro-phenyl)-propylamino]-acetic acid methyl ester [ No CAS ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

17
[ 873-32-5 ]
[ 925-90-6 ]
[ 6323-18-8 ]

Reference： [1]Tetrahedron Letters,2007,vol. 48,p. 7448 - 7451
[2]Chemistry - A European Journal,2005,vol. 11,p. 6889 - 6904

18
[ 201230-82-2 ]
[ 6323-18-8 ]
[ 4767-62-8 ]

Reference： [1]Chemistry - A European Journal,2005,vol. 11,p. 6889 - 6904

19
[ 6323-18-8 ]
[ 1576-35-8 ]
[ 767288-70-0 ]
2-chloropiophenone 4-methylphenylsulfonylhydrazone [ No CAS ]

Reference： [1]Tetrahedron,2007,vol. 63,p. 2695 - 2711

20
[ 6486-05-1 ]
[ 6323-18-8 ]
[ 6512-85-2 ]

Reference： [1]Tetrahedron Letters,2007,vol. 48,p. 7448 - 7451

21
[ 6323-18-8 ]
3-ethyl-1-(4-methylphenylsulfonyl)indazole [ No CAS ]

Reference： [1]Tetrahedron,2007,vol. 63,p. 2695 - 2711

22
[ 89-98-5 ]
[ 6323-18-8 ]

Reference： [1]Tetrahedron,2007,vol. 63,p. 2695 - 2711

23
[ 6323-18-8 ]
[ 40023-85-6 ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

24
[ 6323-18-8 ]
[ 847448-02-6 ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

25
[ 6323-18-8 ]
3-[1-(2-chloro-phenyl)-propyl]-2-mercapto-3<i>H</i>-imidazole-4-carboxylic acid methyl ester [ No CAS ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

26
[ 6323-18-8 ]
Sodium; (E)-2-[1-(2-chloro-phenyl)-propyl]-formyl-amino}-2-methoxycarbonyl-ethenolate [ No CAS ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2005,vol. 15,p. 497 - 500

27
[ 89-98-5 ]
(+-)-piperoin [ No CAS ]
[ 6323-18-8 ]

Reference： [1]Journal of Organic Chemistry,2003,vol. 68,p. 1594 - 1596

28
[ 6323-18-8 ]
[ 81671-56-9 ]

Reference： [1]Journal of Organic Chemistry,1982,vol. 47,p. 2795 - 2798

29
[ 6323-18-8 ]
[ 81671-54-7 ]

Reference： [1]Journal of Organic Chemistry,1982,vol. 47,p. 2795 - 2798

30
[ 6323-18-8 ]
[ 344336-96-5 ]

Reference： [1]Journal of Organic Chemistry,1982,vol. 47,p. 2795 - 2798

31
[ 6323-18-8 ]
[ 90919-30-5 ]

Reference： [1]Journal fur praktische Chemie (Leipzig 1954),1963,vol. 22,p. 202 - 213

32
[ 6323-18-8 ]
[ 37610-57-4 ]

Reference： [1]Journal of Organic Chemistry,1973,vol. 38,p. 835 - 838

33
[ 6323-18-8 ]
[ 35996-56-6 ]

Reference： [1]Journal of Organic Chemistry,1973,vol. 38,p. 835 - 838
[2]Tetrahedron,1978,vol. 34,p. 1627 - 1631

34
[ 6323-18-8 ]
[ 37610-58-5 ]

Reference： [1]Journal of Organic Chemistry,1973,vol. 38,p. 835 - 838

35
[ 6323-18-8 ]
[ 37610-59-6 ]

Reference： [1]Journal of Organic Chemistry,1973,vol. 38,p. 835 - 838

36
[ 6323-18-8 ]
[ 65240-55-3 ]

Reference： [1]Tetrahedron,1978,vol. 34,p. 1627 - 1631

37
[ 6323-18-8 ]
[ 213381-42-1 ]

Yield	Reaction Conditions	Operation in experiment
	With hydrogenchloride; sodium hydroxide; formaldehyd; sulfuric acid; In dichloromethane; water;	1. 7-Chloro-2-methyl-1-indanone (1) 50 g (0.3 mol) of <strong>[6323-18-8]2-<strong>[6323-18-8]chloropropiophenone</strong></strong> (B. L. Jenson et al., Tetrahedron, 1978, 1627) together with 24.55 ml (0.33) of 37% strength formaldehyde solution were placed in the reaction vessel. A solution of 12 g of sodium hydroxide in 600 ml of water was added thereto. The mixture was stirred for 2.5 hours at 40 C. The phases were separated, the aqueous phase was extracted 3 times with 50 ml each time of methylene chloride, the combined organic phases were washed with 100 ml of 1N HCl solution and dried over magnesium sulfate. The methylene chloride solution was added while stirring to 400 g of hot (65 C.) concentrated sulfuric acid over a period of 2.25 hours. The methylene chloride distilled off during this procedure. After the addition was complete, stirring was continued for another 0.5 hour at 65 C. At room temperature, the cool sulfuric acid solution was slowly added to an ice-cold mixture of 325 ml of methylene chloride and 325 ml of water. The phases were separated, the sulfuric acid solution was extracted twice with 250 ml each time of methylene chloride, the combined organic phases were washed with 200 ml of saturated sodium hydrogencarbonate solution, 200 ml of water and 200 ml of saturated sodium chloride solution and dried over magnesium sulfate. After removal of the solvent, the brown liquid was distilled via a 10 cm Vigreux column with column head under a full oil pump vacuum. This gave 39.6 g of (1) as a pale yellow liquid which slowly crystallized. B.p.: 95-98 C (0.3-0.25 mbar); m.p.: 42-43 C.; 1H-NMR (300 MHz, CDCl3): 7.41 (t, 1H), 7.28 (m, 1H), 7.22 (m, 1H), 3.31 (m, 1H), 2.59-2.27 (m, 2H), 1.25 (d, J =7.3 Hz, 3H).

Reference： [1]Patent: US6492539,2002,B1

38
potassium bicarbonate [ No CAS ]
[ 6323-18-8 ]
[ 4865-75-2 ]

Yield	Reaction Conditions	Operation in experiment
	With nitric acid; In water;	EXAMPLE 97 2-Chloro-5-nitropropiophenone 31 ml of 100% nitric acid (dl.52) are introduced into the reaction vessel, and 6 g of <strong>[6323-18-8]o-<strong>[6323-18-8]chloropropiophenone</strong></strong> are added dropwise at -10 C. in the course of 15 minutes in such a way that the reaction temperature is between -5 C. and -10 C. To complete the reaction, stirring is continued at 0 C. for 45 minutes. The reaction mixture is subsequently poured onto 300 g of ice, and the aqueous mixture is extracted twice using 200 ml portions of diethyl ether. The organic phase is washed with 100 ml of water, twice with 100 ml portions of 2N potassium hydrogen carbonate solution and finally with saturated sodium chloride solution, dried over magnesium sulfate and concentrated. The residue is recrystallized from diisopropyl ether/n-hexane; m.p.: 55-56 C.

Reference： [1]Patent: US5336663,1994,A

39
[ 873-32-5 ]
[ 6323-18-8 ]
[ 75815-22-4 ]

Yield	Reaction Conditions	Operation in experiment
		EXAMPLE 5 2-Bromo-2'-chloropropiophenone The procedure of Example 4 is used, except that 16.51 g of 2-chlorobenzonitrile are used instead of 3-chlorobenzonitrile. The 2'-chloropropiophenone obtained after extraction with ethyl acetate is a brown oil which distils under a pressure of about 2.6 kPa and at a temperature of 120 C. About 11.0 g thereof are collected and subjected to bromination as described in Example 4. 26.3 g of a yellow oil are finally obtained, which is used as such in a subsequent step.

Reference： [1]Patent: US4690931,1987,A

40
[ 6323-18-8 ]
[ 18776-12-0 ]

Yield	Reaction Conditions	Operation in experiment
	With sodium borohydrid; In methanol; water;	EXAMPLE 1 Preparation of N-methyl-3-phenyl-3-(2-chlorophenoxy)propylamine hydrochloride A 10.80 g portion of <strong>[6323-18-8]chloropropiophenone</strong> was dissolved in 100 ml of methanol in a 500 ml, 3 necked, round-bottomed flask. The flash was fitted with a nitrogen inlet and a thermometer. The reaction mixture was stirred via magnetic stirring rod, and was held under an atmosphere of nitrogen. While the mixture was cooled in an ice bath, 2.03 g of sodium borohydride was added very slowly. The mixture was removed from the ice bath and then stirred for approximately two hours at room temperature. The mixture was then evaporated to a yellow oil and diluted with approximately 100 ml of water. The mixture was extracted from the water by washing three times with ether. The ether was then washed two times with water and one time with saturated sodium chloride solution. The resulting mixture was dried over sodium sulfate and evaporated to 11.2 g of yellow intermediate product comprising 3-chloro-1-phenyl-1-propanol. A 5.07 g portion of the above intermediate was placed into a 3-necked, 250 ml round-bottomed flask which had been flushed with nitrogen. The flask was fitted with a thermometer, a nitrogen inlet and an addition funnel.

Reference： [1]Patent: EP591584,1994,A1

41
[ 1295-35-8 ]
[ 6323-18-8 ]
[ 594-09-2 ]
[ 897400-48-5 ]

Reference： [1]Organometallics,2006,vol. 25,p. 3124 - 3129

42
[ 1295-35-8 ]
[ 6323-18-8 ]
[ 672-66-2 ]
[ 897400-50-9 ]

Reference： [1]Organometallics,2006,vol. 25,p. 3124 - 3129

43
[ 6323-18-8 ]
[ 158635-38-2 ]

Reference： [1]Tetrahedron Asymmetry,2008,vol. 19,p. 1992 - 1997

44
[ 6323-18-8 ]
[ 672-66-2 ]
Ni(P(CH₃)2C₆H₅)2(C₆H₄COCHCH₃) [ No CAS ]

Reference： [1]Organometallics,2006,vol. 25,p. 3124 - 3129

45
[ 6323-18-8 ]
[ 557-20-0 ]
(R)-1-(2-chlorophenyl)propanol [ No CAS ]
[ 158635-38-2 ]

Reference： [1]Synthesis,2012,vol. 44,p. 2162 - 2172

46
[ 6323-18-8 ]
[ 1972-28-7 ]
[ 1469875-61-3 ]
C₁₅H₁₉ClN₂O₅ [ No CAS ]

Reference： [1]Bulletin of the Korean Chemical Society,2013,vol. 34,p. 1955 - 1956

47
[ 67-56-1 ]
[ 6323-18-8 ]
[ 5408-59-3 ]

Reference： [1]Chemistry - A European Journal,2015,vol. 21,p. 3576 - 3579

48
[ 6323-18-8 ]
(6-(2-ethylsulfonylphenyl)-5-methyl-2-trifluoromethyl)imidazo[2,1-b][1,3,4]thiadiazole [ No CAS ]

Reference： [1]Patent: WO2015/91945,2015,A1

49
[ 6323-18-8 ]
1-(2-ethylsulfonylphenyl)propan-1-one [ No CAS ]

Reference： [1]Patent: WO2015/91945,2015,A1

50
[ 6323-18-8 ]
2-bromo-1-(2-ethylsulfonylphenyl)propan-1-one [ No CAS ]

Reference： [1]Patent: WO2015/91945,2015,A1

51
[ 6323-18-8 ]
[ 811-51-8 ]
1-(2-ethylsulfanylphenyl)propan-1-one [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
1.95 g	In N,N-dimethyl-formamide; at 0 - 40℃; for 2h;	To a solution of <strong>[6323-18-8]1-(2-chlorophenyl)propan-1-one</strong> (20.0 g, 1 18.6 mmol) in N,N-dimethyl-formamide (100 ml) at 0-5C was added sodium ethanethiolate (24.9 g, 296.5 mmol). The suspension was warmed to room temperature, then stirred at 40C for 2 hours. The reaction mixture was poured on saturated aqueous ammonium chloride, extracted with ethyl acetate, the combined organic layers were washed with water and brine, dried over sodium sulfate and evaporated to dryness. The residue was dissolved in diethyl ether, the solution treated with activated charcoal, stirred, filtered over hyflo and the solvent evaporated in vacuo. The product was precipitated from n-heptane at 10C, filtered and dried to afford a first crop (16.8 g). The mother liquor was concentrated, and the residue purified by chromatography on silica gel (n-heptane/dichloromethane 2:1 ) to further deliver 1.95 g of product as a pale yellow solid, mp 30-31 C. LCMS (method ZCQ13): 195 (M+H)+, retention time 1.53 min.

Reference： [1]Patent: WO2015/91945,2015,A1 .Location in patent: Page/Page column 50; 51

52
[ 6323-18-8 ]
C₁₃H₁₄ClN₃S [ No CAS ]

Reference： [1]MedChemComm,2016,vol. 7,p. 1441 - 1448

53
[ 6323-18-8 ]
C₁₀H₁₀ClN₃S [ No CAS ]

Reference： [1]MedChemComm,2016,vol. 7,p. 1441 - 1448

54
[ 6323-18-8 ]
(E)-5-methyl-4-(2-chlorophenyl)-2-(((2-carboxyl)benzylidene)hydrazinyl)thiazole [ No CAS ]

Reference： [1]MedChemComm,2016,vol. 7,p. 1441 - 1448

55
[ 6323-18-8 ]
(E)-5-methyl-4-phenyl-2-(1-methyl-2-((4-methyl)-(2-carboxyl)benzylidene)hydrazinyl)thiazole [ No CAS ]

Reference： [1]MedChemComm,2016,vol. 7,p. 1441 - 1448

56
[ 110-89-4 ]
[ 6323-18-8 ]
2-piperidin-1-[(3-(chlorophenyl))]propan-1-one [ No CAS ]

Reference： [1]Journal of Organic Chemistry,2016,vol. 81,p. 11565 - 11573

57
[ 6323-18-8 ]
[ 87-48-9 ]
6-bromo-2-(2-chlorophenyl)-3-methylquinoline-4-carboxylic acid [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
		1.00 g (4.42 mmol) of 5-bromo-1H-indole-2,3-dione was initially charged in 12.0 ml of acetic acid, and 746 mg (4.42 mmol) of <strong>[6323-18-8]1-(2-chlorophenyl)propan-1-one</strong> were added. The reaction mixture was stirred at 75 C. for 5 min. Subsequently, 4.0 ml of concentrated hydrochloric acid were added, and the mixture was stirred at 105 C. overnight. After cooling to RT, the reaction mixture was added to 200 ml of 1 M hydrochloric acid. The precipitated solid was then filtered off, washed with water and dried under reduced pressure. This gave 1.07 g (40% of theory; purity 63%) of the title compound. LC/MS (Method 1, ESIpos): Rt=0.94 min, m/z=376/378 [M+H]+.

Reference： [1]Patent: US2018/36300,2018,A1 .Location in patent: Paragraph 0404-0406

58
[ 6323-18-8 ]
methyl 4-([6-bromo-2-(2-chlorophenyl)-3-methylquinolin-4-yl]carbonyl}amino)bicyclo[2.2.2]octane-1-carboxylate [ No CAS ]

Reference： [1]Patent: US2018/36300,2018,A1

59
[ 6323-18-8 ]
4-([6-bromo-2-(2-chlorophenyl)-3-methylquinolin-4-yl]carbonyl}amino)bicyclo[2.2.2]octane-1-carboxylic acid [ No CAS ]

Reference： [1]Patent: US2018/36300,2018,A1

60
[ 6323-18-8 ]
[ 103-49-1 ]
(E)-1-(2-chlorophenyl)-2-methyl-3-phenylprop-2-en-1-one [ No CAS ]

Reference： [1]Chemistry - A European Journal,2018,vol. 24,p. 17027 - 17032

61
[ 6323-18-8 ]
[ 103-49-1 ]
2-benzyl-3-(2-chlorophenyl)-2-methyl-3-oxopropanenitrile [ No CAS ]

Reference： [1]Chemistry - A European Journal,2018,vol. 24,p. 17027 - 17032

62
sesquiethylaluminum chloride dimer [ No CAS ]
[ 609-65-4 ]
[ 6323-18-8 ]

Yield	Reaction Conditions	Operation in experiment
	With aluminium trichloride; at 40℃;	Hereinafter there are listed examples of ketones obtainalbe or obtained by the process of the invention: hexanone-3 decanone-4 ... 3-methoxyacetophenone 3-phenoxyacetophenone o-chloroacetophenone o-chloropropiophenone m-chloroacetophenone 3-chloro-5-methylpropiophenone 2,6-dichloroacetophenone ...

Reference： [1]Patent: US4266066,1981,A

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Ghs Precautionary Statements

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Code	Phrase
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P103	Read label before use
Prevention
Code	Phrase
P201	Obtain special instructions before use.
P202	Do not handle until all safety precautions have been read and understood.
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P211	Do not spray on an open flame or other ignition source.
P220	Keep/Store away from clothing/combustible materials.
P221	Take any precaution to avoid mixing with combustibles
P222	Do not allow contact with air.
P223	Keep away from any possible contact with water, because of violent reaction and possible flash fire.
P230	Keep wetted
P231	Handle under inert gas.
P232	Protect from moisture.
P233	Keep container tightly closed.
P234	Keep only in original container.
P235	Keep cool
P240	Ground/bond container and receiving equipment.
P241	Use explosion-proof electrical/ventilating/lighting/equipment.
P242	Use only non-sparking tools.
P243	Take precautionary measures against static discharge.
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P261	Avoid breathing dust/fume/gas/mist/vapours/spray.
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P272	Contaminated work clothing should not be allowed out of the workplace.
P273	Avoid release to the environment.
P280	Wear protective gloves/protective clothing/eye protection/face protection.
P281	Use personal protective equipment as required.
P282	Wear cold insulating gloves/face shield/eye protection.
P283	Wear fire/flame resistant/retardant clothing.
P284	Wear respiratory protection.
P285	In case of inadequate ventilation wear respiratory protection.
P231 + P232	Handle under inert gas. Protect from moisture.
P235 + P410	Keep cool. Protect from sunlight.
Response
Code	Phrase
P301	IF SWALLOWED:
P304	IF INHALED:
P305	IF IN EYES:
P306	IF ON CLOTHING:
P307	IF exposed:
P308	IF exposed or concerned:
P309	IF exposed or if you feel unwell:
P310	Immediately call a POISON CENTER or doctor/physician.
P311	Call a POISON CENTER or doctor/physician.
P312	Call a POISON CENTER or doctor/physician if you feel unwell.
P313	Get medical advice/attention.
P314	Get medical advice/attention if you feel unwell.
P315	Get immediate medical advice/attention.
P320
P302 + P352	IF ON SKIN: wash with plenty of soap and water.
P321
P322
P330	Rinse mouth.
P331	Do NOT induce vomiting.
P332	IF SKIN irritation occurs:
P333	If skin irritation or rash occurs:
P334	Immerse in cool water/wrap n wet bandages.
P335	Brush off loose particles from skin.
P336	Thaw frosted parts with lukewarm water. Do not rub affected area.
P337	If eye irritation persists:
P338	Remove contact lenses, if present and easy to do. Continue rinsing.
P340	Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P341	If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
P360	Rinse immediately contaminated clothing and skin with plenty of water before removing clothes.
P361	Remove/Take off immediately all contaminated clothing.
P362	Take off contaminated clothing and wash before reuse.
P363	Wash contaminated clothing before reuse.
P370	In case of fire:
P371	In case of major fire and large quantities:
P372	Explosion risk in case of fire.
P373	DO NOT fight fire when fire reaches explosives.
P374	Fight fire with normal precautions from a reasonable distance.
P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
P377	Leaking gas fire: Do not extinguish, unless leak can be stopped safely.
P378
P380	Evacuate area.
P381	Eliminate all ignition sources if safe to do so.
P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
Storage
Code	Phrase
P401
P402	Store in a dry place.
P403	Store in a well-ventilated place.
P404	Store in a closed container.
P405	Store locked up.
P406	Store in corrosive resistant/ container with a resistant inner liner.
P407	Maintain air gap between stacks/pallets.
P410	Protect from sunlight.
P411
P412	Do not expose to temperatures exceeding 50 oC/ 122 oF.
P413
P420	Store away from other materials.
P422
P402 + P404	Store in a dry place. Store in a closed container.
P403 + P233	Store in a well-ventilated place. Keep container tightly closed.
P403 + P235	Store in a well-ventilated place. Keep cool.
P410 + P403	Protect from sunlight. Store in a well-ventilated place.
P410 + P412	Protect from sunlight. Do not expose to temperatures exceeding 50 oC/122oF.
P411 + P235	Keep cool.
Disposal
Code	Phrase
P501	Dispose of contents/container to ...
P502	Refer to manufacturer/supplier for information on recovery/recycling

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Physical hazards
Code	Phrase
H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
H350	May cause cancer
H351	Suspected of causing cancer
H360	May damage fertility or the unborn child
H361	Suspected of damaging fertility or the unborn child
H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 6323-18-8 ] {[proInfo.proName]}

Quality Control of [ 6323-18-8 ]

Related Doc. of [ 6323-18-8 ]

Product Details of [ 6323-18-8 ]

Safety of [ 6323-18-8 ]

Application In Synthesis of [ 6323-18-8 ]

[ 6323-18-8 ] Synthesis Path-Upstream 1~11

[ 6323-18-8 ] Synthesis Path-Downstream 1~62

Related Functional Groups of [ 6323-18-8 ]

Aryls

Chlorides

Ketones

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

Inquiry

Related Functional Groups of
[ 6323-18-8 ]