Alternatived Products of [ 65000-12-6 ]
Product Details of [ 65000-12-6 ]
CAS No. : | 65000-12-6 |
MDL No. : | MFCD09800968 |
Formula : |
C10H14BrNO2S
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Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
292.19
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Pubchem ID : | - |
Synonyms : |
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Application In Synthesis of [ 65000-12-6 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 65000-12-6 ]
- 1
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[ 680183-37-3 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
77% |
With bromine In dichloromethane for 3h; Heating; |
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- 2
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[ 65000-12-6 ]
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[ 18640-74-9 ]
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N,N-diethyl-2-(2-isobutylthiazol-5-yl)benzenesulfonamide
[ No CAS ]
- 3
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[ 1192-58-1 ]
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[ 65000-12-6 ]
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[ 1454889-71-4 ]
Yield | Reaction Conditions | Operation in experiment |
41% |
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 130℃; for 20h; Inert atmosphere; Schlenk technique; regioselective reaction; |
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- 4
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[ 1455-20-5 ]
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[ 65000-12-6 ]
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N,N-diethyl-2-(5-butylthiophen-2-yl)benzenesulfonamide
[ No CAS ]
- 5
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[ 4208-57-5 ]
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[ 65000-12-6 ]
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[ 1454889-70-3 ]
Yield | Reaction Conditions | Operation in experiment |
82% |
With potassium acetate; palladium diacetate In N,N-dimethyl acetamide at 130℃; for 20h; Inert atmosphere; Schlenk technique; regioselective reaction; |
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- 6
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[ 2905-25-1 ]
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[ 109-89-7 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
95% |
With triethylamine In dichloromethane at 20℃; for 1h; |
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67% |
With triethylamine In dichloromethane at 0 - 20℃; for 12h; Schlenk technique; Inert atmosphere; |
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Reference:
[1]Okumura, Shogo; Nakao, Yoshiaki
[Organic Letters, 2017, vol. 19, # 3, p. 584 - 587]
[2]Bheeter, Charles B.; Jin, Rongwei; Bera, Jitendra K.; Dixneuf, Pierre H.; Doucet, Henri
[Advanced Synthesis and Catalysis, 2014, vol. 356, # 1, p. 119 - 124]
- 7
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[ 65000-12-6 ]
-
[ 65000-18-2 ]
Yield | Reaction Conditions | Operation in experiment |
42% |
With palladium diacetate; potassium pivalate In N,N-dimethyl acetamide at 150℃; for 16h; Schlenk technique; Inert atmosphere; |
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- 8
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[ 108-86-1 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 2 steps
1: chlorosulfonic acid / Schlenk technique; Inert atmosphere
2: triethylamine / dichloromethane / 12 h / 0 - 20 °C / Schlenk technique; Inert atmosphere |
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- 9
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[ 615-36-1 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
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Multi-step reaction with 2 steps
1.1: hydrogenchloride; sodium nitrite / water / 0 °C
1.2: 0 - 20 °C
2.1: sulfur dioxide; copper dichloride / acetonitrile / 18 h / 70 °C / Inert atmosphere; Schlenk technique |
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- 10
-
[ 1319750-41-8 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
37% |
With sulfur dioxide; copper dichloride In acetonitrile at 70℃; for 18h; Inert atmosphere; Schlenk technique; |
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- 11
-
[ 2905-25-1 ]
-
[ 121-44-8 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
72% |
With sodium sulfate In water at 20℃; for 3.2h; Electrochemical reaction; |
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63% |
With copper(I) oxide; oxygen In 1,2-dichloro-ethane at 50℃; for 4h; Sealed tube; |
|
Reference:
[1]Sheykhan; Khani; Abbasnia; Shaabanzadeh; Joafshan
[Green Chemistry, 2017, vol. 19, # 24, p. 5940 - 5948]
[2]Ji, Jing; Liu, Zhengyi; Liu, Ping; Sun, Peipei
[Organic and Biomolecular Chemistry, 2016, vol. 14, # 29, p. 7018 - 7023]
- 12
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[ 65000-12-6 ]
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[ 5720-05-8 ]
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[ 2059070-88-9 ]
Yield | Reaction Conditions | Operation in experiment |
92% |
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate In ethanol; water at 80℃; for 3h; Inert atmosphere; |
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- 13
-
[ 60199-33-9 ]
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[ 121-44-8 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
70% |
With sodium sulfate In water; acetonitrile at 20℃; for 9h; Electrochemical reaction; |
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- 14
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[ 2905-25-1 ]
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[ 65000-12-6 ]
Yield | Reaction Conditions | Operation in experiment |
|
Multi-step reaction with 2 steps
1: hydrazine hydrate / tetrahydrofuran / 0.25 h / 10 °C
2: sodium sulfate / water; acetonitrile / 9 h / 20 °C / Electrochemical reaction |
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