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Chemical Structure| 6560-72-1 Chemical Structure| 6560-72-1

Structure of 6560-72-1

Chemical Structure| 6560-72-1

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Product Details of [ 6560-72-1 ]

CAS No. :6560-72-1
Formula : C13H19NO
M.W : 205.30
SMILES Code : OC1(C)CN(CC2=CC=CC=C2)CCC1
MDL No. :MFCD22628457

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Application In Synthesis of [ 6560-72-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6560-72-1 ]

[ 6560-72-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 917-54-4 ]
  • [ 50606-58-1 ]
  • [ 6560-72-1 ]
YieldReaction ConditionsOperation in experiment
50% In tetrahydrofuran; diethyl ether; for 3h; N-BENZYLPIPERIDONE (2 g, HCI salt, hydrate) was stirred with THF (20 mL), concentrated to dryness, and placed under high vac. The residue was diluted in THF (20 mL), and methyllithium was added (2.5 eq of 1. 6N in ET20) via syringe. After stirring for 3 hr, the mixture was concentrated in vacuo, diluted with water, extracted with CH2CI2, and dried over NA2SO4. Filtration and concentrating in vacuo gave the desired product (50%, MH+ = 205).
50% N-Benzylpiperidone (2 g, HC1 salt, hydrate) was stirred with THF (20 mL), concentrated to dryness, and placed under high vac. The residue was diluted in THF (20 mL), and methyllithium was added (2.5 eq of 1.6N in Et2O) via syringe. After stirring for 3 hr, the mixture was concentrated in vacuo, diluted with water, extracted with CH2C12, and dried over Na2SO4. Filtration and concentrating in vacuo gave the desired product (50%, MH+=205).
50% In tetrahydrofuran; diethyl ether; for 3h; PREPARATIVE EXAMPLE 2.11; Step A Step B; Step B 0 Step B HO N'H Step A N-Benzylpiperidone (2 g, HCI salt, hydrate) was stirred with THF (20 mL), concentrated to dryness, and placed under high vac. The residue was diluted in THF (20 mL), and methyllithium was added (2.5 eq of 1. 6N in Et2O) via syringe. After stirring for 3 hr, the mixture was concentrated in vacuo, diluted with water, extracted with CH2CI2, and dried over Na2SO4. Filtration and concentrating in vacuo gave the desired product (50%, MH+ = 205).
50% N-Benzylpiperidone (2 g, HCI salt, hydrate) was stirred with THF (20 mL), concentrated to dryness, and placed under high vac. The residue was diluted in THF (20 mL), and methyllithium was added (2.5 eq of 1.6N in Et20) via syringe. After stirring for 3 hr, the mixture was concentrated in vacuo, diluted with water, extracted with CH2CI2, and dried over Na2SO4. Filtration and concentrating in vacuo gave the desired product (50%, MH+ = 205).

 

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