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Chemical Structure| 6590-97-2 Chemical Structure| 6590-97-2

Structure of 6590-97-2

Chemical Structure| 6590-97-2

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Product Details of [ 6590-97-2 ]

CAS No. :6590-97-2
Formula : C7H3Cl2NS
M.W : 204.08
SMILES Code : S=C=NC1=C(Cl)C(Cl)=CC=C1
MDL No. :MFCD00041048
InChI Key :RQZIODPVCCTBAQ-UHFFFAOYSA-N
Pubchem ID :2796281

Safety of [ 6590-97-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P260-P264-P280-P301+P330+P331-P303+P361+P353-P304+P340-P305+P351+P338-P310-P321-P363-P405-P501
Class:8
UN#:1759
Packing Group:

Application In Synthesis of [ 6590-97-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6590-97-2 ]

[ 6590-97-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 921222-14-2 ]
  • [ 6590-97-2 ]
  • [ 921222-15-3 ]
YieldReaction ConditionsOperation in experiment
To a solution of <strong>[921222-14-2]2,3-diamino-6-methylsulfanyl-benzoic acid ethyl ester</strong> (150 mg) in acetonitrile (10 mL) are added 2,3-dichlorophenyl isothiocyanate (98 muL). The reaction mixture obtained is stirred 1 hour at RT and N-(3-dimethylaminopropyl)-N'-ethylcarbodiimide hydro-chloride (EDCI, 166 mg) is added. The mixture obtained is cooled to RT, quenched with H2O and extracted with EtOAc. The organic layers obtained are combined, dried over MgSO4, filtrated and solvent is evaporated to afford the title compound (LC/MS Rt=3.55, [M]+=395.93 and 397.89 and 399.89).
 

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