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Chemical Structure| 6625-74-7 Chemical Structure| 6625-74-7

Structure of N-Phenylpivalamide
CAS No.: 6625-74-7

Chemical Structure| 6625-74-7

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Product Details of [ 6625-74-7 ]

CAS No. :6625-74-7
Formula : C11H15NO
M.W : 177.24
SMILES Code : CC(C)(C)C(=O)NC1=CC=CC=C1
MDL No. :MFCD00043691
InChI Key :LWJNWXYSLBGWDU-UHFFFAOYSA-N
Pubchem ID :81103

Safety of [ 6625-74-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P305+P351+P338-P330-P332+P313-P337+P313-P362-P403+P233-P405-P501

Application In Synthesis of [ 6625-74-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6625-74-7 ]

[ 6625-74-7 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 6625-74-7 ]
  • [ 56619-93-3 ]
  • [ 104-88-1 ]
  • [ 1309448-77-8 ]
  • [ 1351696-87-1 ]
  • 2
  • [ 887144-94-7 ]
  • [ 6625-74-7 ]
  • [ 25617-34-9 ]
  • [ 125686-52-4 ]
  • 3
  • [ 887144-94-7 ]
  • [ 6625-74-7 ]
  • [ 1939-19-1 ]
  • [ 25617-34-9 ]
  • [ 125686-52-4 ]
  • 4
  • [ 6625-74-7 ]
  • [ 65854-91-3 ]
  • [ 62662-74-2 ]
YieldReaction ConditionsOperation in experiment
8.8%; 82.2% With 1,3-bis(1-adamantyl)imidazolium tetrafluoroborate; N-chloro-succinimide; camphor-10-sulfonic acid; In 1,4-dioxane; at 25℃; for 24h; General procedure: A mixture of Acetylaniline (0.2 mmol), NCS (0.26 mmol), D-CSA (0.1 mmol) and 1,3-di(1-adamantl)imidazolium tetrafluoroborate (0.01 mmol) in dioxane (1 mL) wasstirred at room temperature (25 oC) under air atmosphere for 24h. The reactionmonitored by GC-MS. When the acetylaniline was consumed completely, the reactionmixture was quenched with saturated aq. NaHCO3 (4 mL). The resulting mixture wasextracted with EtOAc (4 mL x 3). The organic layer was washed with pure water (4ml x 3). The combined organic layer was dried over anhydrous Na2SO4, filtered andthe solvent was removed under reduced pressure to provide the crude product. Thepurification was performed by flash column chromatography on silica gel.
 

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