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Chemical Structure| 6626-66-0 Chemical Structure| 6626-66-0

Structure of 6626-66-0

Chemical Structure| 6626-66-0

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Product Details of [ 6626-66-0 ]

CAS No. :6626-66-0
Formula : C16H9NO
M.W : 231.25
SMILES Code : O=C1C2=C(C3=NC4=CC=CC=C4C=C31)C=CC=C2

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Application In Synthesis of [ 6626-66-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6626-66-0 ]

[ 6626-66-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6626-66-0 ]
  • [ 902518-11-0 ]
  • C34H22N2O [ No CAS ]
YieldReaction ConditionsOperation in experiment
43% To a 50 ml Schlenk tube was added <strong>[902518-11-0]9-(2-bromophenyl)carbazole</strong> (0.8 mmol, 260 mg) and anhydrous tetrahydrofuran (8 ml). After the mixture was stirred at -78 ° C for 10 minutes, 1.6 M n-butyllithium (0.8 mL) was added dropwise and reacted at -78 ° C for 1 hour. The fragment ketone (185 mg, 0.8 mmol) was dissolved in anhydrous tetrahydrofuran (5 mL), and the mixture was applied to the mixture, and the mixture was applied to the mixture, and the mixture was stirred at -78 ° C for a few minutes and then transferred to room temperature and stirred overnight. Subsequently, the reaction was extracted with a saturated ammonium chloride solution and extracted with ethyl acetate (20 mL×3). The combined organic phase was washed with water, dried over anhydrous sodium sulfate, filtered, concentrated in vacuo, purified through the column to give a solid (164mg, 43percent yield) as a yellow.
 

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