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CAS No. : | 663194-10-3 | MDL No. : | MFCD03861153 |
Formula : | C8H10BrN3O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | AVLAJWPBZJNJDQ-UHFFFAOYSA-N |
M.W : | 244.09 | Pubchem ID : | 45787495 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P280-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H302-H315-H319-H332-H335 | Packing Group: | N/A |
GHS Pictogram: |
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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
87% | With phosphorus(V) oxybromide; In acetonitrile; for 1.0h;Heating / reflux; | 2c) 4- (4-BROMO-PVRIMIDIN-2-VL)-MORPHOLINE A mixture of <strong>[19810-79-8]2-morpholin-4-yl-pyrimidin-4-ol</strong> (6.08 g, 33.6 MMOL) and phosphorus OXYBROMIDE (12.5 g, 43.7 MMOL) in 330 mL MECN is heated to reflux for 1 hour. The reaction is cooled to room temperature, concentrated to half volume, and poured over ice. The resulting mixture is neutralized with a saturated solution of NaHCOs, and then extracted with methylene chloride. The organic phase is washed with saturated NACI (aqueous), dried over ANHYDROUS MGS04, FILTERED, concentrated and dried to an off-white solid (7.11 g, 87%). M+H'= 245.97. H NMR (CDC13) ; a 8.05 (d, 1H), 6.70 (d, 1H), 3.75 (m, 8H). |
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