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Chemical Structure| 66657-42-9 Chemical Structure| 66657-42-9

Structure of 66657-42-9

Chemical Structure| 66657-42-9

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Product Details of [ 66657-42-9 ]

CAS No. :66657-42-9
Formula : C9H8ClNO3S
M.W : 245.68
SMILES Code : O=S(C1=CC2=C(NC(CC2)=O)C=C1)(Cl)=O
MDL No. :MFCD06655638
InChI Key :ICRHXBNAKSHNRD-UHFFFAOYSA-N
Pubchem ID :4962209

Safety of [ 66657-42-9 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H314
Precautionary Statements:P280-P305+P351+P338-P310
Class:8
UN#:3261
Packing Group:

Application In Synthesis of [ 66657-42-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 66657-42-9 ]

[ 66657-42-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 66657-42-9 ]
  • [ 7149-75-9 ]
  • [ 1345822-54-9 ]
YieldReaction ConditionsOperation in experiment
With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 25℃; for 1h;Inert atmosphere; General procedure: Method A: 2-oxo-1,2,3,4-tetrahydroquinoline-6-sulfonyl chloride (.2 g, 0.814 mmol) was dissolved in DMF (2 ml) and 3,4-dimethylaniline (0.118 g, 0.977 mmol) was added followed by the dropwise addition of DIPEA (0.213 ml, 1.221 mmol). The reaction was stirred at RT for 1 h then purified by directly injecting to a Waters.(R). reverse phase purification system.
 

Historical Records

Technical Information

• Acyl Group Substitution • Alkyl Halide Occurrence • Baeyer-Villiger Oxidation • Barbier Coupling Reaction • Baylis-Hillman Reaction • Bucherer-Bergs Reaction • Chan-Lam Coupling Reaction • Clemmensen Reduction • Complex Metal Hydride Reductions • Corey-Bakshi-Shibata (CBS) Reduction • Corey-Chaykovsky Reaction • Fischer Indole Synthesis • General Reactivity • Grignard Reaction • Henry Nitroaldol Reaction • Hiyama Cross-Coupling Reaction • Horner-Wadsworth-Emmons Reaction • Hydride Reductions • Kinetics of Alkyl Halides • Kumada Cross-Coupling Reaction • Lawesson's Reagent • Leuckart-Wallach Reaction • McMurry Coupling • Meerwein-Ponndorf-Verley Reduction • Passerini Reaction • Paternò-Büchi Reaction • Petasis Reaction • Peterson Olefination • Pictet-Spengler Tetrahydroisoquinoline Synthesis • Preparation of Aldehydes and Ketones • Preparation of Amines • Prins Reaction • Reactions of Aldehydes and Ketones • Reactions of Alkyl Halides with Reducing Metals • Reactions of Amines • Reformatsky Reaction • Robinson Annulation • Schlosser Modification of the Wittig Reaction • Schmidt Reaction • Specialized Acylation Reagents-Carbodiimides and Related Reagents • Specialized Acylation Reagents-Ketenes • Stille Coupling • Stobbe Condensation • Substitution and Elimination Reactions of Alkyl Halides • Suzuki Coupling • Tebbe Olefination • Ugi Reaction • Wittig Reaction • Wolff-Kishner Reduction

Categories

Related Functional Groups of
[ 66657-42-9 ]

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Chlorides

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Amides

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Related Parent Nucleus of
[ 66657-42-9 ]

Tetrahydroquinolines

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