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Chemical Structure| 66749-96-0 Chemical Structure| 66749-96-0

Structure of 66749-96-0

Chemical Structure| 66749-96-0

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Product Details of [ 66749-96-0 ]

CAS No. :66749-96-0
Formula : C17H25NO5
M.W : 323.38
SMILES Code : O=CC1=CC=C(N2CCOCCOCCOCCOCC2)C=C1

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Application In Synthesis of [ 66749-96-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 66749-96-0 ]

[ 66749-96-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17919-34-5 ]
  • [ 66749-96-0 ]
  • [ 1609543-05-6 ]
YieldReaction ConditionsOperation in experiment
52.3% With potassium tert-butylate; for 1.5h;Milling; Irradiation; t-BuOK (1.2 g, 10 mmol) and 4-(1, 4, 7, 10-tetraoxa-13-azacyclopentadecyl) benzaldehyde (1 g, 3 mmol) were placed into a dry mortar and milled vigorously for about 90 min under infrared ray lamp, in the process, 4, 4-Bis(diethylphosphonomethyl)biphenyl(1.36 g, 3.0 mmol) was added in batches. After completion of the reaction (monitored by Thin Layer chromatography (TLC)), the mixture was dissolved in Dichloromethane (150 mL). The residual solid was filtered and filtrate was concentrated. Yellow-green needle product (1.24 g, 1.565 mmol) was obtained by recrystallized from dichloromethane. Yield: 52.3%.
 

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