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Chemical Structure| 6764-10-9 Chemical Structure| 6764-10-9

Structure of 6764-10-9

Chemical Structure| 6764-10-9

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Product Details of [ 6764-10-9 ]

CAS No. :6764-10-9
Formula : C12H8ClNO2S
M.W : 265.72
SMILES Code : O=[N+](C1=CC=CC=C1SC2=CC=C(Cl)C=C2)[O-]
MDL No. :MFCD08458408

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Application In Synthesis of [ 6764-10-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 6764-10-9 ]

[ 6764-10-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 6764-10-9 ]
  • [ 14752-66-0 ]
  • [ 245649-77-8 ]
YieldReaction ConditionsOperation in experiment
83% With sodium hydrogensulfite; In water; dimethyl sulfoxide; at 60℃; for 24h; General procedure: A mixture of sodium arylsulfinates (1.0 mmol), nitroarenes (0.5 mmol), NaHSO3 (1.0 mmol), MIL-101(Fe) (10 mg, 8 mol% of Fe) in H2O (2 mL) were stirred at 60 oC for 20 h in a sealed tube. After cooling to room temperature, the aqueous solution was extracted with ethyl acetate (3 × 3 mL), and the combined extract was dried with anhydrous Na2SO4. The solvent was removed, and the crude product was separated by a flash chromatography on a silica gel column to afford the pure product 3.
 

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