Home Cart Sign in  
Chemical Structure| 69445-45-0 Chemical Structure| 69445-45-0

Structure of 69445-45-0

Chemical Structure| 69445-45-0

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 69445-45-0 ]

CAS No. :69445-45-0
Formula : C13H10N2O
M.W : 210.23
SMILES Code : OC1=CC=C2C(N=CN2C3=CC=CC=C3)=C1

Safety of [ 69445-45-0 ]

Application In Synthesis of [ 69445-45-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 69445-45-0 ]

[ 69445-45-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 69445-45-0 ]
  • [ 57616-74-7 ]
  • 5-<3-(4-morpholino)propoxy>-1-phenylbenzimidazole dihydrochloride [ No CAS ]
YieldReaction ConditionsOperation in experiment
Example 39 5-[3-(4-Morpholino)propoxy]-1-phenylbenzimidazole Dihydrochloride by the Method of Scheme 3 Similar reaction of 5-hydroxy-1-phenylbenzimidazole (Example 14) with sodium hydride followed by <strong>[57616-74-7]4-<strong>[57616-74-7](3-chloropropyl)morpholine hydrochloride</strong></strong> gave Example 39 (52%). DiHCl salt: mp (MeOH/Et2 O) dec. above 84 C. (hygroscopic solid). 1 H NMR (D2 O): delta9.42 (s, 1 H, H-2), 7.81-7.74 (m, 5 H, Ph), 7.72 (d, J=9.2 Hz, 1 H, H-7), 7.47 (d, J=2.2 Hz, 1 H, H-4), 7.34 (dd, J=9.2, 2.2 Hz, 1 H, H-6), 4.33 (t, J=5.6 Hz, 2 H, CH2 N+), 4.23 (br d, J=12.9 Hz, 2 H, morpholino CH2 N+), 3.92 (br t, J=12.9 Hz, 2 H, morpholino CH2 N+), 3.70 (br d, J=12.6 Hz, 2 H, morpholino CH2 O), 3.52 (t, J=5.6 Hz, 2 H, CH2 O), 3.36-3.28 (m, 2 H, morpholino CH2 O), 2.42-2.36 (m, 2 H, CH2 CH2 CH2). 13 C NMR: delta160.39 (s), 142.00 (d), 135.93 (s), 134.61 (s), 133.35 (d), 133.14 (d), 128.94 (s), 127.43 (d), 120.08 (d), 116.89 (d), 100.79 (d), 68.65 (t), 66.58 (t), 57.58 (t), 54.62 (t), 25.86 (t). Analysis calculated for C20 H23 N3 O2.2HCl.3.5H2 O requires: C, 50.7; H, 6.7; N, 8.9%. Found: C, 51.1; H, 7.0; N, 8.8%.
 

Historical Records

Technical Information

Categories