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[ CAS No. 70823-04-0 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
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Chemical Structure| 70823-04-0
Chemical Structure| 70823-04-0
Structure of 70823-04-0 * Storage: {[proInfo.prStorage]}
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Product Details of [ 70823-04-0 ]

CAS No. :70823-04-0 MDL No. :MFCD02018257
Formula : C12H17ClO2S Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :260.78 Pubchem ID :-
Synonyms :

Safety of [ 70823-04-0 ]

Signal Word:Danger Class:8
Precautionary Statements:P280-P305+P351+P338-P310 UN#:3261
Hazard Statements:H314 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 70823-04-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 70823-04-0 ]

[ 70823-04-0 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 29841-69-8 ]
  • [ 70823-04-0 ]
  • [ 178422-64-5 ]
YieldReaction ConditionsOperation in experiment
90% With dmap; triethylamine In dichloromethane for 1h; Ambient temperature;
89% With triethylamine In dichloromethane at 0 - 20℃;
  • 2
  • [ 243128-44-1 ]
  • [ 70823-04-0 ]
  • [ 1612259-94-5 ]
YieldReaction ConditionsOperation in experiment
28% With pyridine; at 20 - 30℃; for 48.0h; Example 9 Compound 9: 4-Tert-butyl-2,6-dimethyl-N-[2-methyl-3,5-bis(trifluoromethyl)phenyl]benzenesulfonamide 4-Tert-butyl-2,6-dimethyl-benzenesulfonyl chloride (0.100 g, 0.383 mmol) was added to a solution of 2-methyl-3,5-bis(trifluoromethyl)aniline (0.094 g, 0.387 mmol) in dry pyridine (1 mL). The reaction was capped and stirred at room temperature for 1 day then stirred at 30 C. for 1 day. The reaction was then concentrated under vacuum. To this was added diethyl ether (60 mL) and the mixture was washed with 0.1 N HCl (3*20 mL) followed by 0.1 N NaOH (2*20 mL) then saturated NaCl (2*20 mL). After drying the organic layer over MgSO4, the solution was filtered and concentrated under vacuum. The crude compound was triturated with hexanes (3*10 mL) to afford the title compound (0.051 g, 28% yield). LCMS (M+Na) 490.
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