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Chemical Structure| 7228-47-9 Chemical Structure| 7228-47-9

Structure of 7228-47-9

Chemical Structure| 7228-47-9

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Product Details of [ 7228-47-9 ]

CAS No. :7228-47-9
Formula : C12H12O
M.W : 172.22
SMILES Code : CC(O)C1=CC=C2C=CC=CC2=C1
MDL No. :MFCD00004111
InChI Key :AXRKCRWZRKETCK-UHFFFAOYSA-N
Pubchem ID :98243

Safety of [ 7228-47-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 7228-47-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7228-47-9 ]

[ 7228-47-9 ] Synthesis Path-Downstream   1~3

  • 1
  • [ 7228-47-9 ]
  • [ 56844-12-3 ]
  • 6-bromo-4-(1-(naphthalen-2-yl)ethoxy)thieno[2,3-d]pyrimidine [ No CAS ]
YieldReaction ConditionsOperation in experiment
93% With caesium carbonate; In acetonitrile; for 24h;Inert atmosphere; Reflux; General procedure: 6-Bromo-4-chlorothieno[2,3-d]pyrimidine(5a) (200 mg, 0.802 mmol) was mixed with 1-phenylethanol (2a) (118 mg, 0.962 mmol), Cs2CO3( 313 mg, 0.962 mmol) and acetonitrile (2 mL). The reaction was then stirredunder nitrogen atmosphere at reflux and followed by GC. The mixture was cooledto rt, diluted with EtOAc (40 mL), washed with sat. aq. KHCO3 (20mL), water (2×20 mL) and brine (30 mL). The combined organic fractions weredried over Na2SO4 and concentrated in vacuum. Crudeproduct was absorbed onto Celite 545 and purified by silica gel columnchromatography (n-pentane/EtOAc,6/1). This gave 245 mg (0.730 mmol, 91%) of 6a as an off-white solid.
  • 2
  • [ 7228-47-9 ]
  • [ 22651-87-2 ]
  • [ 27544-18-9 ]
  • (S)-2-iodo-1-(2-naphthyl)ethyl cyclohexanecarboxylate [ No CAS ]
  • 3
  • [ 64-17-5 ]
  • [ 827-54-3 ]
  • [ 766-08-5 ]
  • [ 7228-47-9 ]
  • [ 775-56-4 ]
  • [ 93-08-3 ]
 

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