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[ CAS No. 7462-76-2 ] {[proInfo.proName]}

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Chemical Structure| 7462-76-2
Chemical Structure| 7462-76-2
Structure of 7462-76-2 * Storage: {[proInfo.prStorage]}
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Product Details of [ 7462-76-2 ]

CAS No. :7462-76-2 MDL No. :MFCD06654371
Formula : C8H8ClNO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 169.61 Pubchem ID :-
Synonyms :

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 7462-76-2 ]
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[ 7462-76-2 ] Synthesis Path-Upstream   1~1

  • 1
  • [ 87-65-0 ]
  • [ 527-60-6 ]
  • [ 7462-76-2 ]
  • [ 15307-93-4 ]
YieldReaction ConditionsOperation in experiment
90.75% With sodium hydroxide In water; N,N-dimethyl-formamide; toluene EXAMPLE 1
Preparation of N-phenyl 2,6-dichloroaniline
37.6 g of 2,4,6-trimethyl phenol and 11 g of sodium hydroxide were dissolved in 30 ml of water and mixed with 150 ml of toluene.
The toluene recovered from heating was mixed with 139 ml of N,N-dimethylformamide to obtain a N,N-dimethylformamide solution.
40 g of 2,6-dichlorophenol was dissolved in 130 ml of toluene, followed by the addition of 9.8 g of sodium hydroxide in 20 ml of water, 41.5 g of N-phenyl chloroacetamide and 8.7 ml of N,N-dimethylformamide, and refluxed in a oil bath at 140°-150° C. for 15 h.
The toluene was recovered from the reflux, and mixed with the above N,N-dimethylformamide solution and reacted for 3 h.
Recovering N,N-dimethylformamide from the reacted mixture with distillation under reduced pressure (145°-150° C., 8 mm Hg) resulted in the formation of 53 g of N-phenyl 2,6-dichloroaniline and the product yield was 90.75percent.
Reference: [1] Patent: US5475139, 1995, A,
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