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[ CAS No. 7614-93-9 ] {[proInfo.proName]}

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Chemical Structure| 7614-93-9
Chemical Structure| 7614-93-9
Structure of 7614-93-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 7614-93-9 ]

CAS No. :7614-93-9 MDL No. :N/A
Formula : C16H16 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W :208.30 Pubchem ID :-
Synonyms :

Safety of [ 7614-93-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 7614-93-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7614-93-9 ]

[ 7614-93-9 ] Synthesis Path-Downstream   1~18

  • 2
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YieldReaction ConditionsOperation in experiment
1: 20% 2: 50% With pyridine; bis(triphenylphosphine)nickel(II) chloride; zinc In acetonitrile at 60 - 70℃; for 4h;
  • 4
  • [ 7647-01-0 ]
  • [ 98-86-2 ]
  • after/according to/ Clemmensen amalgamated zinc [ No CAS ]
  • [ 292638-84-7 ]
  • [ 100-41-4 ]
  • [ 7614-93-9 ]
  • [ 1520-44-1 ]
  • 5
  • [ 7647-01-0 ]
  • [ 98-86-2 ]
  • in acidic solution amalgamated zinc [ No CAS ]
  • [ 292638-84-7 ]
  • [ 100-41-4 ]
  • [ 7614-93-9 ]
  • [ 1520-44-1 ]
  • 6
  • [ 100-42-5 ]
  • [ 98-10-2 ]
  • [ 7614-93-9 ]
  • [ 1146-47-0 ]
YieldReaction ConditionsOperation in experiment
84% With C13H17ClN3O2Pd(1-); toluene-4-sulfonic acid In toluene at 100℃; for 18h; chemoselective reaction; General conditions General procedure: to a mixture of 3 (0.25 mmol), 1 (10 mol %), and p-TsOH (5.00 × 10-2 mmol) in a 2 dram vial were added toluene (3 mL) and 2 (0.75 mmol). After stirring for 18 h at 100 °C, the reaction mixture was diluted with CH2Cl2 (3 mL), neutralized with Et3N (5.00 × 10-2 mmol), and filtered through Celite. The resulting solution was concentrated in vacuo then purified using flash column chromatography with silica gel (4:1 hexanes/EtOAc).
1: 52 %Chromat. 2: 45 %Chromat. With 1-butyl-3-methylimidazolium Tetrafluoroborate at 80℃; for 5h;
  • 7
  • [ 7614-93-9 ]
  • [ 13304-62-6 ]
  • [ 1370037-76-5 ]
  • 8
  • [ 292638-84-7 ]
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  • [ 6362-80-7 ]
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  • [ 22768-22-5 ]
  • [ 56763-57-6 ]
  • 9
  • [ 292638-84-7 ]
  • [ 98-83-9 ]
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  • [ 38212-18-9 ]
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  • 10
  • [ 100-42-5 ]
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  • [ 6416-39-3 ]
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  • [ 38212-18-9 ]
  • 4-methyl-2,4-diphenylpent-2-ene [ No CAS ]
  • 2,4-diphenylpent-2-ene [ No CAS ]
YieldReaction ConditionsOperation in experiment
With 10percentwt. zeolite HZSM-12 In chlorobenzene at 120℃; for 5h;
  • 11
  • [ 292638-84-7 ]
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  • 12
  • [ 67-56-1 ]
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  • [ 1414398-15-4 ]
  • 13
  • [ 292638-84-7 ]
  • [ 67-56-1 ]
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  • [ 1520-44-1 ]
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  • 14
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  • 15
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  • 16
  • [ 111-12-6 ]
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  • [ 1431318-10-3 ]
  • 17
  • [ 100-42-5 ]
  • [ 1255944-34-3 ]
  • [ 7614-93-9 ]
  • 1,2-diphenyltricyclo[8.3.1.03,9]tetradec-3(9)-ene [ No CAS ]
  • [ 38661-81-3 ]
  • [ 93-52-7 ]
YieldReaction ConditionsOperation in experiment
1: 60% 2: 44% 3: 42% 4: 4% With silica gel at 50℃; for 12h; 4.5 Acid-catalyzed reaction of 7-bromo-1-phenylcycloheptene (1a) with styrene Compound 1a (4g, 15.9mmol), styrene (1.66g, 15.9mmol), and 0.1g silica gel were stirred at 50°C for 12h. The crude material was purified by column chromatography (hexane) to give 2a (1.63g, 60%), 4 (0.17g, 4%), 5 (1.3g, 44%), 6 (0.7g, 42%). The spectral data for compounds 4, 5, and 6 are consistent with those reported in the literature.11-13 Compound 4: 1H NMR (300MHz, CDCl3) δ 7.41-7.36 (m, 5H), 5.15 (dd, 1H, J=5.6, 10.4Hz), 4.11-3.99 (m, 2H). Compound 5: 1H NMR (300MHz, CDCl3) δ 7.47-7.27 (m, 5H), 5.24 (q, 1H, J=6.9Hz), 2.07 (d, 3H, J=6.9Hz). Compound 6: 1H NMR (300MHz, CDCl3) δ 7.38-7.18 (m, 10H), 6.47-6.35 (m, 2H), 3.70-3.61 (m, 1H), 1.48 (d, 3H, J=7.0Hz).
  • 18
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  • [ 2605-18-7 ]
  • [ 14310-21-5 ]
YieldReaction ConditionsOperation in experiment
84% With bis(1,5-cyclooctadiene)nickel (0); tricyclohexylphosphine In tetrahydrofuran at 80℃; for 12h; Inert atmosphere; Glovebox;
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