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CAS No. : | 7664-66-6 | MDL No. : | MFCD00059188 |
Formula : | C9H13NO | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 151.21 g/mol | Pubchem ID : | 82112 |
Synonyms : |
|
Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P261-P305+P351+P338 | UN#: | N/A |
Hazard Statements: | H315-H319-H335 | Packing Group: | N/A |
GHS Pictogram: |
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Yield | Reaction Conditions | Operation in experiment |
---|---|---|
62% | With sodium hydride In N,N-dimethyl-formamide; mineral oil at 20℃; for 24 h; | General procedure: These syntheses were carried out in one step as per De Marco et al. [24] Aminophenol (92 mmol) and a suspension of NaH in mineral oil (275 mmol NaH) were suspended in dry DMF (100 mL). The corresponding alkylbromide (137 mmol) was added dropwise and the mixture was then stirred for 24 h at room temperature. The reaction was quenched by adding 400 mL of distilled water and the aqueous layer was extracted with 3 × 150 mL of ethyl acetate. Collected organic layers were dried over anhydrous Na2SO4 and concentrated in vacuo. Pure product was obtained by distillation under reduced pressure. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
71% | With hemicucurbituril supported [Bmim]Cl In toluene for 10 h; Reflux | General procedure: A mixture of aryl halide (1 mmol) and sodium alkoxide(3.0 mmol) was refluxed in the presence of 200 mg ofHmCucSILP catalyst in toluene (5 mL) for an appropriatetime as indicated in Table 2. After completion of thereaction, the reaction mixture was filtered and solvent wasevaporated in vacuo to give the crude product, which waspurified by column chromatography over silica gel usinghexane/EtOAc as the eluent. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
73% | With hemicucurbituril supported [Bmim]Cl In toluene for 9 h; Reflux | General procedure: A mixture of aryl halide (1 mmol) and sodium alkoxide(3.0 mmol) was refluxed in the presence of 200 mg ofHmCucSILP catalyst in toluene (5 mL) for an appropriatetime as indicated in Table 2. After completion of thereaction, the reaction mixture was filtered and solvent wasevaporated in vacuo to give the crude product, which waspurified by column chromatography over silica gel usinghexane/EtOAc as the eluent. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With hemicucurbituril supported [Bmim]Cl In toluene for 10 h; Reflux | General procedure: A mixture of aryl halide (1 mmol) and sodium alkoxide(3.0 mmol) was refluxed in the presence of 200 mg ofHmCucSILP catalyst in toluene (5 mL) for an appropriatetime as indicated in Table 2. After completion of thereaction, the reaction mixture was filtered and solvent wasevaporated in vacuo to give the crude product, which waspurified by column chromatography over silica gel usinghexane/EtOAc as the eluent. |
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