Home Cart Sign in  
Chemical Structure| 769-82-4 Chemical Structure| 769-82-4

Structure of 769-82-4

Chemical Structure| 769-82-4

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 769-82-4 ]

CAS No. :769-82-4
Formula : C7H11N3O
M.W : 153.18
SMILES Code : CC1=NC=C(COC)C(N)=N1

Safety of [ 769-82-4 ]

Application In Synthesis of [ 769-82-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 769-82-4 ]

[ 769-82-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 769-82-4 ]
  • [ 2908-71-6 ]
YieldReaction ConditionsOperation in experiment
87% With hydrogen bromide; In acetic acid; at 100℃; S4. Add 100 grams of ring-closing product to a 1-liter jar.Slowly add 500 ml of 33% HBr/HOAc solution.Slowly warm the system to 100C,Maintain this temperature for 8-16 hours,TLC determines the endpoint of the reaction.After the reaction is completed, 20 grams of acidic activated carbon is added while hot, and the mixture is stirred for 30 minutes and then filtered. The filtrate is concentrated under pressure and dried to dryness. 30 milliliters of anhydrous ethanol is added, and the crystals are cooled and filtered.149 g of the target product was dried to give a yield of 87%.
 

Historical Records

Technical Information

Categories