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Structure of 7736-25-6

Chemical Structure| 7736-25-6

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Product Details of [ 7736-25-6 ]

CAS No. :7736-25-6
Formula : C13H13NO2
M.W : 215.25
SMILES Code : O=C1N(CCCC=C)C(C2=C1C=CC=C2)=O
MDL No. :MFCD00957803
InChI Key :BYKYMPVVZNUAEX-UHFFFAOYSA-N
Pubchem ID :339434

Safety of [ 7736-25-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H317
Precautionary Statements:P280-P305+P351+P338

Application In Synthesis of [ 7736-25-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 7736-25-6 ]

[ 7736-25-6 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 7736-25-6 ]
  • [ 14437-03-7 ]
  • [ 1047673-23-3 ]
  • 2
  • [ 7736-25-6 ]
  • [ 14437-03-7 ]
  • [ 1046834-49-4 ]
  • 3
  • [ 67-56-1 ]
  • [ 7736-25-6 ]
  • [ 3728-43-6 ]
  • [ 1234714-96-5 ]
  • 4
  • [ 928-50-7 ]
  • [ 1074-82-4 ]
  • [ 7736-25-6 ]
YieldReaction ConditionsOperation in experiment
98.09% With nickel(II) sulphate; Methyltriphenylphosphonium bromide; In N,N,N,N,N,N-hexamethylphosphoric triamide; at 200℃; for 3h; Equipped with a mechanical stirrer, a reflux condenser and a thermometer 1000ml four-necked flask, followed by adding 50g (0.48mol) 5- chloro-1-pentene, 50g (0.27mol) phthalimide potassium salt, triphenyl phosphine bromide 0.25g, 2.5g and 500g of nickel sulfate, hexamethylphosphoric triamide. After the addition was complete, the oil bath was heated to 200 deg.] C, the reaction was kept for 3 hours. After incubation, cooled to room temperature. Filter cake by-product potassium chloride reactions, polymerization inhibitor and a catalyst. Rinsed with acetone 100ml fresh cake combined filtrate and washings. Under reduced pressure using a rotary evaporator, acetone was distilled off spin, hexamethylphosphoric triamide and the excess of <strong>[928-50-7]5-chloro-1-pentene</strong>. Get 57g red viscous liquid, liquid chromatography measured content of 94.81%, the yield was 98.09%.
 

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[ 7736-25-6 ]

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