Home Cart Sign in  
Chemical Structure| 81787-94-2 Chemical Structure| 81787-94-2

Structure of 81787-94-2

Chemical Structure| 81787-94-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 81787-94-2 ]

CAS No. :81787-94-2
Formula : C16H13NO
M.W : 235.28
SMILES Code : O=CC(N1CC2=CC=CC=C2)=CC3=C1C=CC=C3
MDL No. :MFCD25368408

Safety of [ 81787-94-2 ]

Application In Synthesis of [ 81787-94-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 81787-94-2 ]

[ 81787-94-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 81787-94-2 ]
  • [ 3171-46-8 ]
  • 2-(1-benzyl-1H-indol-2-yl)-4,6-dimethyl-1H-benzo[d]imidazole [ No CAS ]
YieldReaction ConditionsOperation in experiment
68% With triethylamine; In ethanol; for 12.0h;Reflux; General procedure: Compound 4 (1mmol) was taken in dissolved in ethanol in the presence of triethylamine, and appropriate diamine (1mmol). The mixture was refluxed with stirring for 12h and was monitored for completion using TLC. The reaction was generally completed in 12-15h. After the completion of the reaction, excess of ethanol was removed under reduced pressure. The product was extracted using ethyl acetate and organic layer was washed with distilled water. The combined organic layer was dried over anhydrous sodium sulfate, filtered, concentrated and purified by isocratic flash column chromatography (petroleum ether: ethyl acetate=9.5: 0.5, v/v) on silica gel (200-400) to afford pure N-benzylated indole-benzimidazole derivatives (5a-i) in 55-88% yields. The structures were confirmed by IR, NMR and HRMS.
 

Historical Records

Technical Information

Categories